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J <br /> Analytical Data <br /> Client: Hyde Environmental, Inc. Job Number: 720-22819-1 <br /> Client Sample ID: SF-E <br /> Lab Sample ID'. 720-22819-2 Dale Sampled: 09/24/2009 0900 <br /> Client Matrix: Solid Date Received:09/24/2009 1900 <br /> 8270C Semivolatile Compounds by Gas Chromatography/Mass Spectrometry(GC/MS) <br /> Method: 8270C Analysis Batch:720-58779 Instrument ID: SAT 2K2 <br /> Preparation: 3550B Prep Batch:720-58557 Lab File ID: clsatumwstepdatatda <br /> Dilution: 1.0 Initial WeighWolume: 30.14 g <br /> Date Analyzed: 09/30/2009 1400 Final WeighWolume: 1 mL <br /> Date Prepared: 09/ M009 0941 Injection Volume: 1.0 uL <br /> Analyte DryWt Corrected:N Result(mg/Kg) Qualifier RL <br /> Phenanthrene NO 0.067 <br /> Anthracene NO 0.067 <br /> Di-n-butyl phthalate NO 0.17 <br /> Fluoranthene NO 0.067 <br /> Pyrene NO 0.067 <br /> Butyl benzyl phthalate NO 0.17 <br /> 3,3'-Dichlorobenzidine NO 0.17 <br /> Benzo[a]anthracene NO 0.33 <br /> Sis(2-ethylhexyl)phthalate NO 0.33 <br /> Chrysene ND 0.067 <br /> Di-n-oclyl phthalate ND 1.0 <br /> Benzo[b]fluoranthene ND 0.067 <br /> Benzo[a]pyrene ND 0.067 <br /> Benzo[k]fluoranthene ND 0.067 <br /> Indeno[7.2,3-cd]pymne ND 0.067 <br /> Benzo[g,h.i]perylene ND 0.067 <br /> Benzoic acid ND 0.33 <br /> Azobenzene ND 0.067 <br /> Dibenz(a,h)anthracene ND 0.067 <br /> Surrogate %Rec Qualifier Acceptance Limits <br /> Nitrobenzene-d5 68 21 -98 <br /> 2-Fluorobiphenyl 74 38-96 <br /> Terphenyl-dl4 81 32-117 <br /> 2-Fluorophenol 93 28-98 <br /> Phenol-d5 72 23-101 <br /> 2,4,6-Tdbromophenol 75 37-114 <br /> TestAmerica San Francisco Page 32 of 102 10/13/2009 <br />