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J <br /> Analytical Data <br /> Client: Hyde Environmental, Inc. Job Number: 720-22819-1 <br /> Client Sample ID: SF-W <br /> Lab Sample ID: 720-22819-3 Date Sampled 09/24/2009 0930 <br /> Client Matrix: Solid Date Received:09/24/2009 1900 <br /> 8270C Semivolatile Compounds by Gas Chromatography/Mass Spectrometry(GC/MS) <br /> Method: 8270C Analysis Batch:720-58779 Instrument ID: SAT 21<2 <br /> Preparation: 35508 Prep Batch:720-58557 Lab File ID: c:\satumws\epdata\da <br /> Dilution: 2.0 Initial Weight/Volume: 30.16 g <br /> Date Analyzed: 09/30/2009 1747 Final NleightfVolume: 1 ml- <br /> Date <br /> LDate Prepared: 09/29/2009 0941 Injection Volume: 1.0 uL <br /> Analyte DryVA Corrected N Result(mg/Kg) Qualifier RL <br /> Phenanthrene ND 0.13 <br /> Anthracene ND 0.13 <br /> Di-n-butyl phthalate ND 0.34 <br /> Fluoranthene NO 0.13 <br /> Pyrene ND 0.13 <br /> Butyl benzyl phthalate NO 0.34 <br /> 3.3'-Dichlorobenzidine NO 0.34 <br /> Benzo[a]anthracene NO 0.66 <br /> Bis(2ethylhexyl)phthalate NO 0.66 <br /> Chrysene NO 0.13 <br /> Di-n-oclyl phthalate NO 2.0 <br /> Benzo[blfluoranthene NO 0,13 <br /> Benzo[a]pyrene NO 0.13 <br /> Benzo[k]fluoranthene ND 0.13 <br /> Indeno[1,2,3-cd]pyrene NO 0.13 <br /> Benzo(g,h,ilperylene ND 0.13 <br /> Benzoic acid ND 0.66 <br /> Azobenzene ND 0.13 <br /> Dibenz(a,h)anthracene ND 0.13 <br /> Surrogate %Rec Qualifier Acceptance Limits <br /> Nitrobenzene-d5 50 21 -98 <br /> 2-Fluorobiphenyl 66 38-96 <br /> Terphenyl-d14 75 32-117 <br /> 2-Fluorophenol 75 28-98 <br /> Phenol-d5 64 23-101 <br /> 2,4,6-Tdbromophenol 66 37-114 <br /> TestAmen"San Francisco Page 34 of 102 10/13/2009 <br />