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s <br /> Analytical Data <br /> Client: Hyde Environmental, Inc. Job Number: 720-22819-1 <br /> Client Sample ID: B-M(3') <br /> Lab Sample ID: 720-22819-7 Date Sampled: 09/24/2009 1005 <br /> Client Matrix: Solid Date Received:09/24/2009 1900 <br /> 8270C Semivolatile Compounds by Gas Chromatography/Mass Spectrometry(GC/MS) <br /> Method: 8270C Analysis Batch:720-58779 Instrument ID: SAT 2K2 <br /> Preparation: 35508 Prep Batch:720-58557 Lab File ID: c:\satumm\epdata\da <br /> Dilution: 1.0 Initial WeighWolume: 30.02 g <br /> Date Analyzed: 09/30/2009 1610 Final WeighWolume: 1 mL <br /> Date Prepared: 09/29/2009 0941 Injection Volume: 1.0 uL <br /> Analyte Dry\M Corrected:N Result(mg/Kg) Qualifier RL <br /> Phenanthrene NO 0.067 <br /> Anthracene NO 0.067 <br /> Di-n-butyl phthalate NO 0.17 <br /> Fluoranthene ND 0.067 <br /> Pyrene ND 0.067 <br /> Butyl benzyl phthalate NO 0.17 <br /> 3,3'-Dichlorobenzidine NO 0.17 <br /> Benzo(ajanthracene NO 0.33 <br /> Bis(2-ethyl"l)phthalate NO 0.33 <br /> Chrysene NO 0.067 <br /> Di-n-octyl phthalate ND 1.0 <br /> Benzo[b]fluoranthene NO 0.067 <br /> Benzo[a]pyrene ND 0-067 <br /> Benzo[klfluoranthene ND 0.067 <br /> Indeno[1,2,3-od]pyrene NO 0.067 <br /> Benzo[g,h,i]perylene NO 0.067 <br /> Benzoic acid NO 0.33 <br /> Azobenzene NO 0.067 <br /> Dibenz(a,h)anthracene NO 0.067 <br /> Surrogate %Rec Qualifier Acceptance Limits <br /> Nitrobenzene-d5 53 21 -98 <br /> 2-Fluorobiphenyl 65 38-96 <br /> Terphenyl-d14 85 32-117 <br /> 2-Fluorophenol 70 28-98 <br /> Phenol-d5 52 23-101 <br /> 2,4,6-Tnbromophenol 83 37-114 <br /> TestAmerice San Francisco Page 42 of 102 10/13/2009 <br />