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Analytical Data <br /> Client: Hyde Environmental, Inc. Job Number: 720-22819-1 <br /> Client Sample ID: B-S(3') <br /> Lab Sample ID: 720-22819-9 Date Sampled: 09/24/2009 1020 <br /> Client Matrix: Solid Date Received:0924/2009 1900 <br /> 8270C Semivolatile Compounds by Gas ChromatographylMass Spectrometry(GC/MS) <br /> Method: 8270C Analysis Batch:720-58779 Instrument ID: SAT 2K2 <br /> Preparation: 3550B Prep Batch:720-58557 Lab File ID: 0satumvrs\epdata\da <br /> Dilution: 1.0 Initial WeighVVolume: 30.09 9 <br /> Date Analyzed: 09/30/2009 1715 Final Weight/Volume: 1 mL <br /> Date Prepared: 0929/2009 0941 Injection Volume: 1.0 uL <br /> Analyte DryWt Corrected:N Result(mg/Kg) Qualifier RL <br /> Phenanthrene ND 0.067 <br /> Anthracene ND 0.067 <br /> Di-n-butyl phthalate ND 0.17 <br /> Fluoranthene ND 0.067 <br /> Pyrene NO 0.067 <br /> Butyl benzyl phthalate ND 0.17 <br /> 3.3'-Dichlorobenzidine ND 0.17 <br /> Benzo(a)anthracene NO 0.33 <br /> Bis(2-elhylhexyl)phthalate ND 0.33 <br /> Chrysene ND 0.067 <br /> Di-n-octyl phthalate ND 1.0 <br /> Benzo[bjfluorardhene ND 0.067 <br /> Benzo[ajpyrene ND 0.067 <br /> Benzo[k]fluoranthene NO 0.067 <br /> Indeno[1,2,3-cdlpyrene NO 0.067 <br /> Benzolg.h,i)perylene NO 0.067 <br /> Benzoic acid NO 0.33 <br /> Azobenzene ND 0.067 <br /> Dibenz(a.h)anthracene NO 0.067 <br /> Surrogate %Rec Qualifier Acceptance Limits <br /> Nitrobenzene-d5 50 21-98 <br /> 2-Fluorobiphenyl 55 38-96 <br /> Terphenyl-d14 63 32-117 <br /> 2-Fluorophenol 63 28-98 <br /> Phenol-05 51 23-101 <br /> 2,4,6-Tribromophenol 62 37-114 <br /> TestAmerica San Francisco Page 46 of 102 10/13/2009 <br />