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Analytical Data <br /> Client: Hyde Environmental, Inc. Job Number: 720.22819-1 <br /> Client Sample ID: SOIL PILE <br /> Lab Sample ID: 720-22819-10 Date Sampled: 09/24/2009 1030 <br /> Client Matrix: Solid Date Received:0924/2009 1900 <br /> 8270C Semivolatile Compounds by Gas Chromatogrsphy/Maas Spectrometry(GC/MS) <br /> Method 8270C Analysis Batch:720-58779 Instrument ID: SAT 2K2 <br /> Preparation: 35508 Prep Batch:720-58557 Lab File ID: c:lsalumwslepdatalda <br /> Dilution: 2.0 Initial WeightlVolume: 30.10 g <br /> Date Analyzed: 09/30/2009 1820 Final WeightlVolume: 1 mL <br /> Date Prepared: 0929/2009 0941 Injection Volume: 1.0 UL <br /> Analyte DryM Corrected. N Result(mg/Kg) Qualifier RL <br /> Phenarrthrene ND 0.13 <br /> Anthracene NO 0.13 <br /> Di-n-butyl phthalate NO 0.34 <br /> Fluoranthene ND 0.13 <br /> Pyrene ND 0.13 <br /> Butyl benzyl phthalate NO 0.34 <br /> 3,3'-Dichlorobenzidine NO 0,34 <br /> Benzo[a]anthracene NO 0.66 <br /> Bis(2ethylhexyl)phthalate ND 0.68 <br /> Chrysene ND 0.13 <br /> Di-n-octyl phthalate ND 2.0 <br /> Benzo[b]fluoranthene NO 0.13 <br /> Benzo[a]pyrene NO 0.13 <br /> Benzo[k]fluoranthene ND 0.13 <br /> Indeno[1,2.3-cd]pyrene ND 0.13 <br /> Benzo[g,h,i]perylene ND 0.13 <br /> Benzoic acid ND 0.66 <br /> Azobenzene ND 0.13 <br /> Dibenz(a,h)anthracene NO 0.13 <br /> Surrogate %Rec Qualifier Acceptance Limits <br /> Nitrobenzene-d5 46 21 -98 <br /> 2-Fluorobiphenyl 65 38-96 <br /> Terphenyl-dl4 71 32-117 <br /> 2-Fluorophenol 75 28-98 <br /> Phenol-d5 58 23-101 <br /> 2.4,6-Tdbromophenol 73 37-114 <br /> TestAmedca San Francisco Page 48 of 102 10/13/2009 <br />