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Quality Control Results <br /> Client: Hyde Environmental, Inc. Job Number: 720-22819-1 <br /> Matrix Spike/ Method:8260B <br /> Matrix Spike Duplicate Recovery Report-Batch: 720-58522 Preparation:50308 <br /> MS Lab Sample ID: 720-22819-2 Analysis Batch: 720-58423 Instrument ID: Chenstation 3 <br /> Client Matrix: Solid Prep Batch: 720-58522 Lab File ID: 09260915.10 <br /> Dilution: 1.0 Initial WeightNolume: 5.26 g <br /> Date Analyzed: 0926/20091558 Final Weight/Volume: 10 mL <br /> Date Prepared: 0926/2009 0800 <br /> MSD Lab Sample ID: 720-22819-2 Analysis Batch: 720-58423 Instrument ID: Chenstation 3 <br /> Client Matrix: Solid Prep Batch: 720-58522 Lab File ID: 09260916.D <br /> Dilution: 1.0 Initial WeighWolume: 5.58 g <br /> Date Analyzed: 0926/20091630 Final WeighWolume: 10 mL <br /> Date Prepared: 09/26/2009 0800 <br /> Analyte MS MSD Limit RPD RPD Limit MS Qual MSD Qual <br /> Methyl tert-butyl ether 97 103 69-130 1 20 <br /> Acetone 89 98 37-150 4 20 <br /> Benzene 97 101 70-130 2 20 <br /> Dichlorobromomelhane 102 109 64-135 0 20 <br /> Bromobenzene 101 105 70-130 2 20 <br /> Chlorobromomethane 98 104 65-130 1 20 <br /> Bromoform 100 107 58-132 0 20 <br /> Bromomethane 96 100 56-130 1 20 <br /> 2-Butanone(MEK) 100 107 41 -150 1 20 <br /> n-Bulylbenzene 103 107 60-145 3 20 <br /> sec-Butylbenzene 102 105 64-137 3 20 <br /> tert-Butylbenzene 104 108 63-134 2 20 <br /> Carbon disulfide 96 100 10-150 2 20 <br /> Carbon tetrachloride 99 105 54-130 0 20 <br /> Chlorobenzene 101 105 70-130 1 20 <br /> Chloroethane 103 102 61 -130 7 20 <br /> Chloroform 99 104 67-130 1 20 <br /> Chloromethane 94 101 50-131 1 20 <br /> 2-Chlorotoluene 104 110 70-130 1 20 <br /> 4-Chlorotoluene 103 108 70-130 1 20 <br /> Chlorodibromomethane 102 110 60-141 1 20 <br /> 1,2-Dichlorobenzene 101 105 70-130 2 20 <br /> 1,3-Dichlorobenzene 100 105 70-130 2 20 <br /> 1,4-Dichlorobenzene 99 103 70-130 2 20 <br /> 1,3-Dichloropropane 101 107 70-130 0 20 <br /> 1,1-Dichloropropene 103 108 67-130 1 20 <br /> 1,2-Dibromo-3-Chloropropane 104 108 57-130 3 20 <br /> Ethylene Dibromide 99 105 66-135 0 20 <br /> Dibromomethane 98 105 65-131 1 20 <br /> Calculations are performed before rounding to avoid round-off errors in calculated results. <br /> TestAmerica San Francisco Page 67 of 102 10/13/2009 <br />