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Quality Control Results <br /> Client: Hyde Environmental, Inc. Job Number: 720-22819-1 <br /> Matrix Spike/ Method:8260B <br /> Matrix Spike Duplicate Recovery Report-Batch: 720.58736 Preparation:5030B <br /> MS Lab Sample ID: 720-22819-8 Analysis Batch: 720-58549 Instrument ID: Chenstation 3 <br /> Client Matrix: Solid Prep Batch: 720-58736 Lab File ID: 09290913.D <br /> Dilution: 1.0 Initial Weight/Volume: 5.17 g <br /> Date Analyzed: 09/29/2009 1428 Final WeighWolume: 10 mL <br /> Date Prepared: 0929/2009 0800 <br /> MSD Lab Sample ID: 720-22819-8 Analysis Batch: 720-58549 Instrument ID: Chenstation 3 <br /> Client Matrix: Solid Prep Batch: 720-58736 Lab File ID: 09290914.D <br /> Dilution: 1.0 Initial WeighWolume: 5.16 g <br /> Date Analyzed: 0929/2009 1501 Final WeighWolume: 10 mL <br /> Date Prepared: 0929/2009 0800 <br /> %Rec. <br /> Analyte MS MSD Limit RPD RPD Limit MS Qua] MSD Qual <br /> Methyl tert-butyl ether 318 94 69-130 109 20 F F <br /> Acetone 467 182 37-150 71 20 F F <br /> Benzene 279 94 70-130 99 20 F F <br /> Dichlorobromomethane 309 90 64-135 110 20 F F <br /> Bromobenzene 311 110 70-130 95 20 F F <br /> Chlorobromomethane 285 87 65-130 106 20 F F <br /> Bromoform 336 107 58-132 103 20 F F <br /> Bromomethane 282 101 56-130 94 20 F F <br /> 2-Butanone(MEK) 447 152 41 -150 98 20 F F <br /> n-Butylbenzene 334 130 60-145 87 20 F F <br /> sec-Butylbenzene 342 143 64-137 82 20 F F <br /> tert-Butylbenzene 353 144 63-134 84 20 F F <br /> Carbon disulfide 290 106 10-150 93 20 F F <br /> Carbon tetrachloride 325 116 54-130 95 20 F F <br /> Chlorobenzene 261 98 70-130 91 20 F F <br /> Chloroethane 309 116 61-130 91 20 F F <br /> Chloroform 280 73 67-130 70 20 F F <br /> Chloromethane 292 109 50-131 91 20 F F <br /> 2-Ch]orotoluene 328 126 70-130 89 20 F F <br /> 4-Chlorotoluene 318 119 70-130 91 20 F F <br /> Chlorodibromomethane 330 90 60-141 115 20 F F <br /> 1,2-Dichlorobenzene 289 100 70-130 97 20 F F <br /> 1,3-Dichlorobenzene 283 101 70-130 95 20 F F <br /> 1,4-Dichlorobenzene 277 98 70-130 95 20 F F <br /> 1,3-Dichloropropane 324 95 70-130 109 20 F F <br /> 1,1-Dichloropropene 321 116 67-130 94 20 F F <br /> 12-Dibromo-3-Chloropropane 490 193 57-130 87 20 F F <br /> Ethylene Dibromide 327 98 66-135 108 20 F F <br /> Dibromomethane 317 96 65-131 107 20 F F <br /> Calculations are performed before rounding to avoid round-oft erors in calculated results. <br /> TestAmerica San Francisco page 75 of 102 10/13/2009 <br />