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Quality Control Results <br /> Client Hyde Environmental, Inc. Job Number: 720.22819-1 <br /> Matrix Spike/ Method:82608 <br /> Matrix Spike Duplicate Recovery Report-Batch: 720-58736 Preparation: 50308 <br /> MS Lab Sample ID: 720.22819-8 Analysis Batch: 720-58549 Instrument ID: Chenstation 3 <br /> Client Matrix: Solid Prep Batch: 720-58736 Lab File ID: 09290913.D <br /> Dilution: 1.0 Initial Weight/Volume: 5.17 g <br /> Date Analyzed: 09129/2009 1428 Final WeightlVolume: 10 mL <br /> Dale Prepared: 09129/2009 0800 <br /> MSO Lab Sample ID: 720-22819-8 Analysis Batch. 720-58549 Instrument ID: Chenstation 3 <br /> Client Matrix: Solid Prep Batch: 720-58736 Lab File ID: 09290914.D <br /> Dilution: 1.0 Initial Weight/Volume: 5.16 9 <br /> Date Analyzed: 09/29/2009 1501 Final WeighWolume: 10 mL <br /> Date Prepared: 09/29/2009 0800 <br /> b Rec, <br /> Analyte MS MSD Limit RPD RPD Limit MS Dual MSD Dual <br /> 1,2,3-Tddlloropmpane 485 170 62-150 96 20 F F <br /> 1,1,2-Trichloro-1,2,2-trifluorcethane 310 121 52-130 88 20 F F <br /> 1,2,4-Trimethylbenzene 341 127 64-140 91 20 F F <br /> 1,3,5-Tnm thytbenzene 347 135 67-134 88 20 F F <br /> Vinyl acetate 16 0 52-150 NC 20 F F <br /> Vinyl chloride 304 121 62-130 86 20 F F <br /> 2,2-Dichloropropane 327 113 63-130 97 20 F F <br /> Surrogate MS%Rec MSD%Rec Acceptance Urnits <br /> 4-Bromofluorobenzene 92 94 52-130 <br /> 1,2-Dichloroethane-d4(Surr) 111 100 67-132 <br /> Toluene-d8(Surr) 102 99 58-130 <br /> Calculations are performed before rounding to avoid round-off errors in calculated results. <br /> TestAmerica Sen Francisco Page 77 of 102 10/13/2009 <br />