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Quality Control Results <br /> Client: Hyde Environmental, Inc. Job Number: 720-22819-1 <br /> Method Blank-Batch: 720-58557 Method: 8270C <br /> Preparation:35508 <br /> Lab Sample ID: MB 720-58557/1-A Analysis Batch: 720-58620 Instrument ID: Ion Trap <br /> Client Matrix: Solid Prep Batch: 720-58557 Lab File ID: MB 720-715220 9-29-2009 <br /> Dilution: 1.0 Units: mg/Kg Ini0al Weight/Vo]ume: 30.05 g <br /> Date Analyzed: 09/29/2009 2001 Final Weight/Volume: 1 mL <br /> Date Prepared: 09/29/2009 0941 Injection Volume: 1.0 uL <br /> Analyte Result Qua] RL <br /> 2-Methyl-4,6-dinihophenol --- NO 0.33 <br /> N-Nitrosodiphenylamine NO 0.067 <br /> 4-Bromophenyl phenyl ether NO 0.17 <br /> Hexachlorobenzene NO 0.067 <br /> Pentachlorophenol NO 0.33 <br /> Phenanthrene NO 0.067 <br /> Anthracene NO 0.067 <br /> Di-n-butyl phthalate NO 0.17 <br /> Fluoranthene ND 0.067 <br /> Pyrene NO 0.067 <br /> Butyl benzyl phthalate NO 0.17 <br /> 3,3'-Dichlorobenzidine NO 0.17 <br /> Benzo[a]anthracene NO 0.33 <br /> Bis(2-ethylhexyl)phthalate ND 0.33 <br /> Chrysene ND 0.067 <br /> Di-n-octyl phthalate NO 1.0 <br /> Benzo[b]8uoranthene NO 0.067 <br /> Benzo[a]pyrene NO 0.067 <br /> Benzo[k]0uoranthene NO 0.057 <br /> Indeno[1,2,3-od]pyrene NO 0.087 <br /> Benzo[g,h,i]perylene NO 0.067 <br /> Benzoic acid NO 0.33 <br /> Azobenzene NO 0.067 <br /> Dibenz(a,h)anthracene NO 0.067 <br /> Surrogate %Rec Acceptance Limits <br /> Nitrobenzene-d5 78 21-98 <br /> 2-Fluorobipherryl 68 38-96 <br /> Terphenyl-d14 75 32-117 <br /> 2-Fluorophenol 64 28-98 <br /> Phenol-:15 61 23-101 <br /> 2,4,6-Tribromophenol 77 37-114 <br /> Calculations are performed before rounding to avoid round-off errors in calculated results. <br /> TestAnnerica San Francisco Page 79 of 102 10/13/2009 <br />