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Reouestor <br />Address: <br />Sampling Location: <br />California Department of Toxic Substances Control <br />For ECL No.s AU02819 <br />Environmental Chemistry Laboratory <br />to AU02822 <br />700 Heinz Avenue Suite 100. Berkeley, CA 94710. Ph (510) 540-3003 <br />OL <br />Laboratory Report For...TPH-Olasel and Motor Oil <br />Auth. No. t0EC0152-5 <br />Page 1 <br />mg/Kg <br />of 3 <br />Wan Clark <br />Date Collected: 21012011 <br />8800 Cal Comer Ddve <br />Date Received by Lab: 2/11/2011 <br />Sacramento. CA, 9 <br />Date Extracted: 9/20/2011 <br />PH: n -C22 to nC32 calculated <br />as Mohr C <br />Data Analyzed: 4/42011 <br />500 <br />Extraction Method: EPA 3580A <br />Analysis Method: ECL 516-M <br />OAKLAND SAG <br />635 Auaa <br />Stoektork CA <br />Extraction Holding Time Mel 7: NO <br />Analysis Holding Time Met?: yes <br />Extraction Methods: EPA 35100 For aqueous samples: Separatory funnel extraction with methylene chloride. <br />EPA 35508 For solid samples: sonication extraction with methylene chloride <br />EPA 3546 For solid samples: Microwave extraction with methylene chloride. <br />EPA 3580A For oils 8 organic liquid samples; Solvent dilution with methylene chloride <br />Analytical Method: ECL 816-M Analysis by DB -1 megabors capillary column, GC/FID. <br />ECL Number: —> <br />I AU02821 Method <br />ollector's Sample a <br />Oak 83 blank <br />OL <br />Sample Matrix: <br />Ink Sowem <br />Units: <br />mg/Kg <br />mg/Kg <br />ri <br />Compound CAS e <br />TPH: n -CIO to n -C25 caleulaled <br />as Diesal <br />ND <br />ND <br />100 <br />PH: n -C22 to nC32 calculated <br />as Mohr C <br />NO NO <br />500 <br />Note: OL = Quantitation Limit = Lowest calibration standard x dilution factor <br />NO - Not detected or detected but below half OL D = Detected but below OL NA = Not Analyzed NT=Nontargat peak <br />Comments <br />Soma hydrocarbon peaks are present in both Diesel and Motor Oil Range region but the chromatographic peak pattern does nol exactly match <br />to that of a Diesel and Motor Oil standard. The sample has the charateristirs of a used oil. <br />Analyzed by Joe Acedillo <br />Reviewed by: Carol Wortham <br />Approved by. John Quinn <br />I Il It <br />Date: <br />u IJ• <br />Date: <br />41, ( /X -t I 1 <br />Date: <br />