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March 147 2016 Lab ID : STK1632163 <br /> G&S Enterprise Customer : 3-17751 <br /> Quality Control-Inorganic <br /> onstiluent Melbas <br /> DatW1D Type Units C9nc. QC Dao OQO Note <br /> etala <br /> ilvcr 3050 (CC 1680647-D02) MSD m e <br /> gtkg 40.00 118/a 75.125 <br /> MSRPD mg/kg 40.00 1.6% S20 <br /> PDS m k 40.00 116% 75-125 <br /> allium 3050 03A19/16;202723amb Blank mg/kg ND G1.5 <br /> LCs mg/kg 40.00 95.5% 85-115 <br /> (CC 1680647- MS mg/kg 40.00 166% 75-125 <br /> 002) MSD nsglkg 40.00 105% 75-125 <br /> MSRPD mg/kg 40.00 0.6% 520 <br /> ranadium 3050 PDS m /k 40,00 101% 75-125 <br /> /16:202723amh Hlank mg/kg ND .5 <br /> L.CS mg/kg 40.00 96.3% 85-it$ <br /> 'MS inglkg 40.00 107% 75-125 <br /> (CC 1680647-002) MSD mg/kg 40.00 105% 75.125 <br /> MSRPD mg/kg 40,00 1.9% 520 <br /> PDS mg/kit mg/kit40.00 101% 75-125 <br /> 3050 03/09/16c202723amb Blank mg/kg ND <I <br /> LCS mg/kg 40.00 95.7% 85.115 <br /> MS mg/kg 40.00 107°/a 75.125 <br /> (CC 1680647-002) MSD mg/kg 40.00 105% 75-125 <br /> MSRPD mg/kg 40.00 1,8% 520 <br /> P nasAk 40.00 102% 75-125 <br /> mercury 7471 03/O4/16:2026764c Blank mg/kg ND ; <br /> LCS mg/kg 02500 96.4% 85.115 <br /> (SP 1602049-001 MSD Ms mg/kg 0,2500 83.A% 75-]25 <br /> MgAg 02500 84,4% 75-125 <br /> MSRpb MA&g 0.2500 0.7% 90 <br /> rsevic RCRA 03114/16:202925AC PxBik AWL. -0.0279 0.05 <br /> PDS m L 8.000 118% 75-125 <br /> hromium RCRA 03/14/16202925AC BxBlk mgt 0.0021 .05 <br /> PDS L B.Ow 106% i5d2S <br /> -upper RCRA 00114l16:202925AC lixBlk mg/L 7.0036 0.05 <br /> PDS 8.000 I I 1% 75.125 <br /> LND : <br /> R 03/14/16: 02925AC BxlSlk mg/L 0,0041 0.05PDS m L 8.000 109% 75-125m RCRA 03l14/16;202925AC 6xBlk mg/L 0.029 0.1PDSm L 8,000 120% 75-125tion :PDS faded,matrix-Post Digestion Spike(PDS)W Within Acceptance Range(AR)because of matrix interfaenxg afra,[ing thisanalyte.Data was accepted based m1 the LCS recovery. <br /> :Condnulug Calibmdon Verification-Amlyted to verify the instrument Calibration i5 within criteria.:Continuing Calibration Blank-Anab7A0 verify[be inatrument baseline is Within criteria.:Method Blank-Prepared to verify that 1119 preparation process is not contributing contamination m the samples.:TCLP/STLC Extmetion Blank-prepared to verify shat the preparation process is tint contributing contamination to the eampks,:laboratory Control Smndard/Samplc-Pnparad to verify that the preparation prot;m is not affecting analyte recovery,:Matrix Spikes-A randomsample isspiked with a known amount of analvte.The recoveriex arc an indication of how that samplematrix affects analyte recovery, <br /> :Matrix Spike Duplicate OfMS/MSD pair-A random sample duplicate is spiked with a known amount of analysed.The recoveriesam an indication of how that aamplo matrix affects analyte recovery+MS/MSDRelalive Percent Difference(RPD)-The MS relative percent difference ism indication ofpteeision far the preparation <br /> and analysis. <br /> :Non-denies,Rends was below the DQD gated fr the analyte. <br /> :Data uali 04Cctivc-'Ibis is NC Criteria against which the quaii!X control data is sore arcs. <br /> Page 14 of 18 <br />