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March 14,2016 Lab ID : STK1632163 G& S Enterprise Customer A-17751 Quality Control-Inorganic wstitueat Method DktelrD Type Units Coo, QC Dan DQO Note Metals Nickel 200.7 03/09116203394AC CCB PPM -0.0007 0.01 20.7 03/14/162,03567AC CCV PPM 1.000 102°A 90-110 CCD PPID 0.0014 0.01 CCV ppm IAM 101°% 90-110 CCB Porn 0.0009 0.01 Sclmium 20.7 03/09!]6203394AC CCV PPM 1700 95.9% 90-110 CCB PPM 0.0020 0.01 CCV ppm 1.000 94.1% 90-110 CCE PRM 0.0009 1 0.01 2 .7 03/14/16:203567AC CCV ppm LOM 99.1% 90.!10 CCB Ppm 0.094 0.01 CCV PPM IAO 98.3% 90-110 CCB m 0.0013 0.01 i1..« 20.7 03/0/16203394AC CCV ppm L000 0Q20$ 900.0L0 CCB pp CCV Pp1n 1.00 109% 90-110 CCB m 0.016 0.01 AIGum 200.7 03/09/16:203394AC CCV ppm 1.000 98.1% 90-110 �B Ppm -0.005 OAI CCV ppm IA0 96.3% 90-110 CCB ppm -0.002 0.01 anadium 20.7 63MJ 16203394AC CCV ppm 1.000 97.6% 90.110 CCB PPM 4.0003 0.01 CCV ppm 1.00 95.8% 90-110 CCB PPM -0.0002 0.01 inc 20.7 0310/16203394AC CCV Ppm 1.00 99.5 ak 90-I IO CCB PPM -0.002 0.62 CCV ppm 1.00 96.4% 90.110 CCQ PPM -0.002 0.02 2451 03/07/16203198AC CCV ppb 4,00 104% 90-110 ercury CCB ppb -0.2 20 CCV PPb 4.0M 104% 90-110 CCB ppb .0.2 20 odMony 3050 03/09/16:202733amb Blank mglkg NU <0'5 LCs mg(kg 24.0 97.2% 85-115 MS mg/kg 24.0 98.3% 75-125 (CC 1680647-002) MSD mg/kg 24.00 99.3% 75.125 MSR.PD mg/kg 40.0 0.03% S20 PDS 24.00 9812% 75-125 3050 03/09116:202723amb BWdc mg/kg ND <0.5 seoic LCs Mg/kg 40.00 93.4% 85-115 009 mg/kg 40.0 105% 75-125 (CC 1680647-002) MSD mg/kg 40.00 105% 75-125 MSAPD mgfkg 40.00 U5% 510 PDS m 40.00 101% 75-125 uim„ 3050 03/09716:202723amb Blank mg/kg000 84.9% 85-1I3 LCs mg/kg MS mg/kg 40.0 1034/. 75-125 (CC 1690647-002) MMSD SRpD mg/k40.0 O 1% 7�S PDS 40.00 99.7% 75125 esyylli9m 3050 03/09/16202723amb Blank Mg/kgND <0.3 LCs mg/kg 40.00 95.8% 85-115 MS M h 40.0 109% 75.125 Page 12 of 18