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November 20, 2001 Lab ID STK135508 <br />Advanced Interconnect Tech. Customer: 3-3147 <br />Quality Control - Inorganic <br />Constituent <br />Method <br />Date/ID <br />Type <br />Units <br />Conc. <br />QC Data <br />DQO <br />Note <br />Metals <br />Zinc <br />3010A <br />11/08/2001:B207 <br />PDS <br />mg/L <br />0.8000 <br />102% <br />75-125 <br />MS <br />mg/L <br />0.8000 <br />106% <br />75-125 <br />(SP 110406-01) <br />mg/L <br />0.8000 <br />1 <br />MMSD <br />SRPD <br />mg/L <br />0.% <br />s20.o <br />200.7 <br />I1/13/2001:B <br />01 -CCB <br />mg/L <br />ND <br /><0.02 <br />01-CCV <br />mg/L <br />0.5000 <br />102% <br />90-110 <br />02 -CCB <br />mg/L <br />NO <br /><0.02 <br />02-CCV <br />mg/L <br />0.5000 <br />99.9% <br />90-110 <br />Wet Chem <br />Cyanide. Total <br />450OCNCE <br />ll/12/2001:A210 <br />Blank <br />mg/L <br />NO <br /><0.01 <br />78-119 <br />LCS <br />mg/L <br />0.1000 <br />109% <br />MS <br />mg/L <br />0.05000 <br />85.7% <br />8-123 <br />(SP 110322-01) <br />MSD <br />mg/L <br />0.05000 <br />91.2%s0 <br />23 <br />MSRPD <br />mg/L <br />Cyanide <br />450OCNCE <br />11/13200LA <br />00 -CCB <br />mg/L <br />0.1000 <br />ND <br />101% <br /><0.01 <br />90-110 <br />00-CCV <br />mg/L <br />01 -CCB <br />mg/L <br />ND <br /><0.01 <br />of-CCV <br />mg/L <br />0.1000 <br />101% <br />90-110 <br />Explanations <br />435 Sample matrix may be affecting this analyte Data was accepted based on the LCS or CCV recovery. <br />Dermitions <br />Blank Method Blank - Prepared to verify that the preparation process is not contributing contamination to the samples. <br />is affecting analyte <br />LCS Laboratory Control Standard/Sample - Prepared to verify that the preparation process not <br />recovery. <br />PDS Post Digestion Spike (ICP/GFAA) <br />is spiked with a known amount of analyte. The recoveries are an indication o <br />MS/MSD Matrix Spikes - A random sample <br />how that sample matrix affects analyte recovery. <br />Continuing Calibration Verification - Analyzed to verify the instrument calibration is within criteria. <br />CCV <br />CCB Continuing Calibration Blank - Analyzed to verify the instrument baseline is within criteria. <br />ND Non -detect - Result was below the DQO listed for the analyte. <br />control dam is compared. <br />DQO Dara Quality Objective - This is the criteria against which the quality <br />STK135508: Quality Control Page 5 <br />