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KIFF <br /> Report Number : 81509 <br /> Analytical LLC Date : 06/12/2012 <br /> Subject : 3 Soil Samples _ -D <br /> Project Name : Tesoro Stockton Terminal <br /> Project Number : 185702499.200.0010 <br /> FEB 16 2016 <br /> ENVIRONMENTAL <br /> Case Narrative HFAITL'RV:r)°nT"r:"r <br /> A version of this report was previously issued on 06/11/2012. This revised version replaces that report. <br /> All soil samples were reported on a total weight (wet weight) basis. <br /> The Method Reporting Limit for Bromodichloromethane has been increased due to the presence of an <br /> interfering compound for sample Composite-2(A,B,C,D). The Method Reporting Limit for <br /> 1,2,3-Trichloropropane has been increased due to the presence of an interfering compound for samples <br /> Composite-2(A,B,C,D) and Composite-3(A,B,C,D). <br /> Matrix Spike/Matrix Spike Duplicate results associated with samples Composite-1(A,B,C,D), <br /> Composite-2(A,B,C,D), and Composite-3(A,B,C,D) for the analyte Antimony were outside of control limits. <br /> This may indicate a bias for the sample that was spiked. Since the LCS recoveries were within control <br /> limits, no data are flagged. <br /> Matrix Spike/Matrix Spike Duplicate results associated with samples Composite-1(A,B,C,D), <br /> Composite-2(A,B,C,D), and Composite-3(A,B,C,D) for the analyte TPH as Diesel were affected by the <br /> analyte concentrations already present in the un-spiked sample. <br /> Matrix Spike/Matrix Spike Duplicate results associated with samples Composite-1(A,B,C,D), <br /> Composite-2(A,B,C,D), and Composite-3(A,B,C,D) for the analyte 1,2,3-Trichlorobenzene were outside of <br /> control limits. This may indicate a bias for the sample that was spiked. Since the LCS recoveries were <br /> within control limits, no data are flagged. <br /> 2795 2nd Street, Suite 300 Davis, CA 95618 530-297-4800 Page 2 of 28 <br />