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�015 3-1 Wi11ow Pas,Road.Pill sbutg,Cil 4.4565.1701 <br /> McCampbell Analytical, Inc. 1'u 1l Free Telephone;(977)252-92621Fav(925)252-9269 <br /> "i1'h[rt Malin,L'ounis" http:,hvnv mmampbelkoml F-mni17 mnin ri:mccampW1.con) <br /> Glossary of Terms & Qualifier Definitions <br /> Client: Ponder Environmental Services <br /> Project: 17-16039,Pacific Ethanol Spill <br /> WorkOrder: 1701 D08 <br /> AnalyticaL_Qualifiers <br /> H samples were analyzed out of holding time <br /> S surrogate spike recovery outside accepted recovery limits <br /> at sample diluted due to matrix interference <br /> a3 sample diluted due to high organic content. <br /> a4 reporting limits raised due to the sample's matrix prohibiting a full volume extraction. <br /> bl aqueous sample that contains greater than—1 vol. %sediment <br /> c2 surrogate recovery outside of the control limits due to matrix interference. <br /> c7 surrogate value diluted out of range <br /> d7 strongly aged gasoline or diesel range compounds are significant in the TPH(g)chromatogram <br /> e2 diesel range compounds are significant; no recognizable pattern <br /> e7 oil range compounds are significant <br /> el 1 stoddard solvent/mineral spirit(7) <br /> Quality Control Qualifiers <br /> F1 MS/MSD recovery andlor RPD is out of acceptance criteria; LCS validates the prep batch. <br /> F2 LCS/LCSD recovery and/or RPD is out of acceptance criteria. <br /> F3 the surrogate standard recovery and/or RPD is outside of acceptance limits. <br /> F1❑ MS1MSD outside control limits. Physical or chemical interferences exist due to sample matrix. <br /> Page 3 of 69 <br />