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McCam befi Analytical, Inc. W4 Willow P' g Road.PittsbuT,CA `91565-1701 <br /> — Toll Frm'relephonc(877)252-9262'I.-I-r.(925)252-9269 <br /> "When Qu[alrr{'CU fells" maimLmcamp6ell,cnm <br /> Quality Control Report <br /> Client: Ponder Environmental Services WorkGrder: 1701 D08 <br /> Date Prepared: 1131117 Batch]D: 133427 <br /> Date Analyzed: 113 1/17-21111 7 Extraction Method: SW5030B <br /> Instrument: GC10,LCIS Analytical Method: SW8260B <br /> Matrix: Soil Unit: mg/kg <br /> Project: 17-16039;Pacific Ethanol Spill Sample ID: MBILCS-133427 <br /> 1701 D36-026AMSIMSD <br /> QC Summary Report for SW8260B <br /> Analyte MB LCS RL SPK MB SS LCS LCS <br /> Result Result Val °I REC %REC Limits <br /> 1,1-Dichloropropene NO - 0.0050 - <br /> cis-1,3-Dichloropropene NO - 0.4050 - - <br /> trans-1,3-Dichloropropene NO - U050 - - <br /> Diisopropyl ether(D(PE) NO 0.0370 0.0050 0.050 ra 52-129 <br /> Ethylbenzene NO - 0.0050 - - - <br /> Ethyl tert-butyl ether(ETBE) NO 0.0376 D.0050 0,050 - 75 53-125 <br /> Freon 113 ND - 0.0050 - - - - <br /> Hexachlorohutadiene NO - 0.0050 - - - <br /> Hexachloroethane NO - 0.0050 - - - - <br /> 2-Hexanone ND - 0.0050 - - - - <br /> Isopropylbenzene NO - 0.0050 - - - <br /> 4-Isopropyl toluene NO - 0.0050 <br /> Methyl-t-butyl ether(MTBE) NO 0.0382 0.0050 0.050 - 76 58-122 <br /> Methylene chloride NO - 0.0050 - - - <br /> 4-Methyl-2-pentanorte(MIBK) ND - 0,0050 - <br /> Naphthalene NO - 0,0050 - - - - <br /> n-Propyl benzene NO - 0.0050 - - - <br /> Styrene NO - 0.0050 - - - <br /> 1,1,1,2-Tetrachloroethane NO - 0.0050 - - - <br /> 1,1,2,2-Tetrachloroethane NO - 0-0050 - - <br /> Tetrachlorcethene NO - 0-0050 - <br /> Toluene NO 0,0465 0.0050 0.050 - 93 76-130 <br /> 1,2,3-Trichlorobenzene NO - 0,0050 - - - <br /> 1,2,4-Trichlorobenzene NO - 0.0050 - - <br /> 1,1,1-Trichloroethane ND <br /> 1.1,2•Tdchloroethane ND - 0.0050 - - - - - - - <br /> Trichloroethene NO 0.0484 0.0050 onm - 97 72-132 <br /> Trichlorofluoromethane NO - 0.0050 - - - - <br /> 1,2,3-Trichloropropane ND o.0050 - - - <br /> 1,2,4-Trimethylbenzene ND 0.0050 - - - <br /> 1,3,5-Trimethylbenzene NO 0.0050 - <br /> Vinyl Chloride NO - 0.0050 - <br /> Xylenes,Total NO - 0.0050 - - <br /> (Cont.] <br /> NELAP 41D33ORELAP w ' <br /> QAIQC Officer <br /> Page 41 of 69 <br />