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Geotalytical Laboratories, Ioc. <br />1405 Kansas Avenue Modesto, CA 95351 <br />Phone (209) 572-0900 Fax (209) 572.0916 <br />CERTIFICATE <br />OF ANALYSIS <br />Report# K121-07 <br />Oxygenates Date: 5/13/99 <br />Semco project: 99-5029 (Kahlid Massod) Date Rec'd: <br />5/07/99 <br />1217 S 7th Street <br />Date Started: 5/12/99 <br />Date Completed: 5/12/99 <br />Modesto CA 95351 p0# <br />Date Sampled= <br />5/07/99 <br />Sampler. R Azevedo (Geo) <br />Sample ID Lab ID MDL Method <br />Analyte <br />Results Units <br />T1<2 -South ® 15' K21623 10 8260 <br />Methyl tertiary -Butyl Ether (MTBE) <br />NO pg/Kg <br />10 <br />Ethanol <br />ND <br />100 <br />tertiary -Butanol <br />ND <br />10 <br />Di -isopropyl ether (RIPE) <br />ND <br />10 <br />Ethyl tertiary -Butyl Ether (ETBE) <br />ND <br />10 <br />tertlary-Amyl Methyl Ether (TAME) <br />ND <br />TK2-North ® 15' K21624 10 8260 <br />Methyl tertiary -Butyl Ether (MTBE) <br />740 pg/Kg <br />10 <br />Ethanol <br />ND <br />100 <br />tertiary -Butanol <br />2000 <br />10 <br />Di -isopropyl ether (DIPS) <br />ND <br />10 <br />Ethyl tertiary -Butyl Ether (ELBE) <br />NO <br />10 <br />tertiary -Amyl Methyl Ether (TAME) <br />ND <br />TKI-South 0 12' K216Z6 2000 8260 <br />Methyl tertiary -Butyl Ether (MTBE) <br />160000 pg/Kg <br />2000 <br />Ethanol <br />ND <br />20000 <br />tertiary-Butanal <br />NO <br />2000 <br />Di -isopropyl ether (DIPE) <br />ND <br />2000 <br />Ethyl tertiary -Butyl Ether (ETRE) <br />ND <br />2000 <br />tertiary -Amyl Methyl Ether (TAME) <br />ND <br />TKl-North ® 12' K21621 500 8260 <br />lvlethyl tertiary -Butyl Ether (MTBE) <br />31000 pg/Kg <br />500 <br />Ethanol <br />ND <br />5000 <br />tertiary -Butanol <br />ND <br />500 <br />Di -isopropyl ether (DIPE) <br />ND <br />50o <br />Ethyl tertiary -Butyl Ether (ETBE) <br />ND <br />500 <br />tertiary -Amyl Methyl Ether (TAME) <br />ND <br />Dispenser#I Q4' West K21629 10 8260 <br />Methyl tertiary -Butyl Ether (MTBE) <br />NO V9/Kg <br />10 <br />Ethanol <br />ND <br />100 <br />tertiary -Butanol <br />ND <br />10 <br />owsopropyl ether (DIPE) <br />ND <br />10 <br />Ethyl tertiary -Butyl Ether (ETBE) <br />ND <br />10 <br />tertiary -Amyl Methyl Ether (TAME) <br />ND <br />