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Barry H. Nicholson _ CERTIFICATE OF ANALYSIS <br /> Port of Stockton Friday,January 29, 1999 <br /> 2201 W. Washington St. :3 r=�R <br /> Stockton CA. 95205 <br /> a <br /> rO � <br /> Sample Information 0- <br /> Sample <br /> Sample ID: PE4139-02 Sample Type: Grab <br /> Sample Description: Tank#7 Soils Project Name: Site#7 p <br /> Date/Time Sampled: 1/5/99 2:00:00 PM Sample Matrix: Soils , <br /> ANALYTICAL RESULT µ QAIQCREPORT <br /> Date LCS Spike MS Spike <br /> Test Parameter Method DLR Unit Result Dilution Analyzed Blank Cone. LCS% Conc. MS <br /> MSD RSD% <br /> Lead (Pb) EPA 6020 1 mg/kg 1.25 19_�� ND 20 85.5% 20 90.0%__ 8990°/ 0.3% <br /> Benzene EPA 8260 20 ug/Kg NO 1 V..4 NO 10 95.0% 10 95.0% 92.0% 0.8% <br /> Toluene -_� -_ EPA 8260 20 ug/Kg NO 1 NO 10 92.0% 10 90.0°/ 91-0% 0.3 <br /> -- <br /> o-Xylene EPA 8260 20 ug/Kg NO 1 NO 10 9330% 10 91.0% 90.0% 0.3% <br /> Ethylbenzene EPA 8260 20 ug/Kg NO 1 ( NO 10 92.0% 10 96.0% 91.0% 1.3% <br /> 10 92.0% 94.0% 0.5% <br /> Methyl t-Butyl Ether(MtBE) EPA8260 0.005 mg/Kg ND 1 NO 10 99.0% <br /> ND 10 100.0% 10 98.0% 99.0% 0.3% <br /> Diisopropyl ether(DIPE) EPA8260 0.005 mg/Kg NO 1 �p <br /> 5---- ND 10 910% 10 94.0% 95.0% 0.3% <br /> Ethyl-t-butyl ether(ETBE) EPA8260 0.005 mg/Kg NO 1 i.) _ _ _„ <br /> ND 0% 10 96.0% 96.0% 0.0% <br /> Tert-amyl methyl ether(TAME) EPA8260 0.005 mg/Kg NO 1 10 97 <br /> _0 <br /> t-Butanol (TBA) EPA8260 0.05 mg/Kg NO 1 NO 10 90.0% 10 94.0% 95.0% 0.3% <br /> TPN-Gas EPA8260 0.5 mg/Kg NO 1 NO 1~_p98.0% 1 99.0% 97.0% 0.5% <br /> p. <br /> Page 1 of 2 <br /> EPA-Em m..."n(nl Prosection Agent}'HfeUiod. <br /> SM-Slarulard Method for Examination of N4aer Wasteivater 18th Ed. <br />