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RECEIVE <br /> FEB 2 6 2014 <br /> • QCBatchlD:QC1143o59 Analyst lucy Method: EPA 82608 <br /> Matrix: Solid Analyzed: 01/13/2014 Instrument: VOA-MS(group) ENVIRONMENTAL <br /> Blank <br /> Analyte Result Units j ROL Notes <br /> QC1143059MB1 <br /> Hexachlorobutadiene NO ugIK9 5 <br /> Isopropylbenzene __.. .. ND ug/Kg .. ._ _. <br /> m and p-Xylene _ NO ug/Kg <br /> Methylene chloride NO ug/Kg 5 <br /> Methyl-t-butyl Ether(MTBE) NO ._ ugIK9 5 <br /> Naphthalene NO ug/Kg 5 _. <br /> N butylbenzene NO ug/Kg 5 _. <br /> N-propylbenzene. ND ug/Kg _ 5 <br /> NO ug/Kg 5 <br /> -..._.. <br /> NO ug/Kg 5 <br /> Seo-butylbenzene <br /> Styr <br /> ._,..en.e.._ ..._. NO ug/Kg 5 <br /> _... <br /> t-Butyl alcohol(TBA) NO ugIK9 10 _ <br /> ___.. NO ug/Kg 5 <br /> Tert-amylmethylether(TAME) <br /> .. <br /> Tert-butylbenzene NO ug/Kg 5 <br /> Tet rachloroethene.. ... ... ... NO uglKg 5 _ <br /> Toluene._ _ NO -ug/Kg <br /> TPH Gasoline. NO ug/Kg 100 _. .... <br /> trans-1,2-dichloroethene... _ NO ug/Kg 5_ . ....... _.. <br /> tians-1,3-dichloropropene NO ug/Kg 5 <br /> . . .-_-,.. .. _. . 5. <br /> trans-l,4-dtchlaro-2-butene NO ug/Kg _.. . <br /> ..i--- 5 <br /> Tdclorcethene ND ug/Kg _ <br /> TrichlorofluoromethaneND ug/Kg 5 _ <br /> V nyl Chlonde .. _ <br /> NO ug/K9 5 <br /> Xylenes(fatal) <br /> NO ug/Kg 5 <br /> Lab Control Spike/Lab Control Spike Duplicate Summary <br /> Spike Amount ! Spike Result ,1 Recovenes !i Limits <br /> Analyte LCS LCSD LCS LCSD Unit�OS LCSD RPD %Rec RPD Notes <br /> QC11430691-CS1 <br /> 1,1-Dichloroethene 5047 ugIK9 94 59-172 <br /> Benzene __... 50 54. .. ug/Kg 108.. 62137 -.... <br /> ___ <br /> Chlorobenzene 50 55 u9/Kg 110 60_133 <br /> Methyl-t butyl Ether(MTBE) _ 50 41 ug/Kg 82 62-137 ........_.... <br /> _. <br /> ..__-.-.... 50 56 ug/Kg 112 59139 <br /> Toluene -.. -. . ...--_. <br /> Tri <br /> ....-chlo-_r._ 50 48 ug <br /> _ /Kg 96 66-142. --- --- .--- <br /> Matrix Spike/Matrix Spike Duplicate Summary <br /> Sample Spike Amount Spike Result Recoveries Limits <br /> Analyte IAmounl MS MSD MS MSD Units MS MSD RPD °/Rec RPD Notes <br /> QC1143059MS1,QC1143059MSD1 Source: 334746.003 <br /> 1,1-Dichloroethene NO 50 50 45 43 ug/Kg 90 86 4.5 59-172 22 <br /> Ber¢ene <br /> NO 50 50 47 48 ug/Kg 94. 96 2.1 62-137 24 <br /> Chlorobenzene NO 50 50 49 48 ug/Kg 98 96 2.1 60-133 24 <br /> Methyl-t-butyl Ether(MTBE) NO 50 50 40 38 ug/Kg 80 76 5,1 62-137 21 <br /> Toluene NO 50 50 49 48 ug/Kg 98. 96 2.1 59139 2.1 <br /> Trichloroethene NO 50 50 43 42 ugIK9 86 84 2.4 66-142 21 <br /> ASSOCIATED LABORATORIES Analytical Results Report f <br /> 7181-01 Lab Request 334747,Page 9 of 10 <br />