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110 2nd Avenue South,#D7,Pacheco,CA 94553-5560 <br /> 14 1 McCAMPBELL ANALYTICAL INC. Telephone;925-798-1620 Fax:925-798-1622 <br /> ://www.mccuVbcll.com E-mail:main@mccampbell.com <br /> Advanced GeriEnvironmental Client Project ID:Plymouth Square Date Sampled: 05/21/99 <br /> 4005 North Wilson Way Date Received: 05/26/99 <br /> Stockton,CA 95205 Client Contact:Mike Rauser Date Extracted: 05/26/99 <br /> Client P.O: Date Analyzed: 05/28-05/31/99 <br /> Diesel Range(C10-C23)Extractable Hydrocarbons as Diesel <br /> EPA methods modified 8015,and 3550 or 3510;Cali fomia RWQCB(SF Bay Region)method GCFID(3550)or GCFID(3510) <br /> Lab ID Client ID Matrix TPH(d)+ %Recovery <br /> Surrogate <br /> 11901 T-1 S 25,a,g 108 <br /> 11902 SP-1 S 450,a,g,d 112 <br /> 11903 P-1 S 24,c,g 104 <br /> Reporting Limit unless otherwise W 50 ug/L <br /> stated;ND means not detected above <br /> the reporting limit S 1.0 mg/kg <br /> *water and vapor samples are reported in ug/L,wipe samples in ug/wipe,soil and sludge samples in mg/kg,and all TCLP/STLC/SPLP <br /> extracts in ug/L <br /> "cluttered chromatogram resulting in coeluted surrogate and sample peaks,or;surrogate peak is on elevated baseline,or;surrogate has been <br /> diminished by dilution of original extract. <br /> 'The following descriptions of the TPH chromatogram are cursory in nature and McCampbell Analytical is not responsible for their <br /> interpretation:a)unmodified or weakly modified diesel is significant;b)diesel range compounds are significant;no recognizable pattern;c) <br /> aged diesel?is significant);d)gasoline range compounds are significant;e)medium boiling point pattern that does not match diesel(?);f) <br /> one to a few isolated peaks present;g)oil range compounds are significant; h)lighter than water immiscible sheen is present; i)liquid <br /> sample that contains greater than—5 vol.%sediment. <br /> DHS Certification No. 1644 Edward Hamilton,Lab Director <br />