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110 2nd Avenue South,#D7,Pacheco,CA 94553 <br /> McCAMPBELL ANALYTICAL INC. Tele:510-798-1620 Fax:510-798-1622 <br /> Advanced GeoEnvironmental Client Project ID:Exxon Station Date Sampled:06/06/95 <br /> 1803 West March Lane,Ste.A Date Received:06/07/95 <br /> Stockton,CA 95207 Client Contact:Bob Marty/Mike Flores Date Extracted:06/07/95 <br /> Client P.O: Date Analyzed:06/07-06/09/95 <br /> Diesel Range(CIO-C23)Extractable Hydrocarbons as Diesel* <br /> EPA methods modified 8015 and 3550 or 35M California RW CB SF Ba Re 'on method GCFID 3550 or GCFID 3510 <br /> Lab ID Client ID Matrix TPH(d)+ %Recovery <br /> Surrogate <br /> 53155 Tank 4 PB 8' S 20,g 103 <br /> 53156 Tank 4 SP S 250,g 104 <br /> 53157 Tank 5 PB 8' S 32,a 103 <br /> 53158 Tank 5 SP S 16,g b 104 <br /> Reporting Limit unless other- W 50 ug(L <br /> wise stated;ND means not de- <br /> tected above the reporting limit S 1.0 mg/kg <br /> *water samples are reported in ug/L,soil samples in mg/kg and all TCLP and STLC extracts in mg/L <br /> # cluttered chromatogram resulting in coelutedsurrogate and sample peaks,or; surrogate peak is on elevated <br /> baseline,or;surrogate has been diminished by dilution of original extract. <br /> + The following descriptions of the TPH chromatogram are cursory in nature and McCainpbell Analytical is not <br /> responsible for their interpretation: a) unmodified or weakly modified diesel is signifscant; b) diesel rangge <br /> compounds are significant;no recognvable pattern;c)aged diesel?is si cant);d)gasoline range comp0unds <br /> are significant; e) medium boiling point, astern that does not match lesel(?)- t) one to a few isolated peaks <br /> present;g)oil range compounds are sig cant;h)fighter than water immiscible s)leen is present;i)liquid sample <br /> chat contains greater than— 5 vol.% sediment. <br /> DH S Certification No. 1644 —Edward Hamilton,Lab Director <br />