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07/21/2004 14:23 <br />2095720 GED <br />20 <br />PAGE 05/15 <br />20 <br />20.4 <br />20 <br />19.8 <br />GeoA naiyticai Laboratories, <br />Inc, <br />1405 Kansas Avenue <br />Modesto, CA 95351 Phone (209) 572-0900 Fax (209) 572-0916 ` <br />Report # Q184-08 <br />CERTIFICATE OF ANALYSIS <br />Date: <br />7/12/04 <br />Thorpe Oil <br />Date Reed: <br />7/02/04 <br />PO Box 357 <br />Project: 601 E. Main St. - Stockton <br />Date Started: <br />7/08/04 <br />Lodi CA <br />95241 <br />Date Completed.7/08/04 <br />PO# <br />Date Sampled: <br />7/02/04 <br />Sample IDs SP -1,2 <br />Time: <br />Sampler : R. 8ombaywala (Geo') <br />Lab ID: Q200946,Q200947 <br />Method <br />RL <br />Anal to <br />Results <br />Units <br />8260E <br />5.0 <br />Benzene <br />ND <br />Ag/Kg <br />5.0 <br />Toluene <br />ND <br />5.0 <br />Ethyl Benzene <br />NO <br />5.0 <br />Total Xylenes <br />ND <br />10 <br />Methyl tert-butyl ether (NYSE) <br />ND <br />400 <br />Ethanol <br />ND <br />200 <br />tert-Butanol <br />ND <br />10 <br />di -Isopropyl ether (DIPS) <br />ND <br />10 <br />Ethyl tert-butyl ether (ETRE) <br />ND <br />10 <br />tert-Amyl methyl ether (TAVE) <br />ND <br />Matt Page <br />Chemist <br />Surrogate <br />1,2-Dichloroethane-d, <br />2-Bromo-l-chloropropane <br />4-Bromofluorobenzene <br />Certification ## 1157 <br />Amnt Spiked <br />Arant Rec. <br />20 <br />18.9 <br />20 <br />20.4 <br />20 <br />19.8 <br />% Recovery <br />QC Limit <br />94.5 <br />66-133 <br />102.0 <br />63-139 <br />99.0 <br />64-136 <br />oc__ (JI -V5 <br />Donna Keller <br />Laboratory Director <br />