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P <br />.r <br />Tri -Regional Recommendations <br />Appendix A <br />TABLE #2 RECOMMENDED MINIMUM VERIFICATION ANALYSES <br />FOR UNDERGROUND STORAGE TAMW wvFCTir_Ann.Jc <br />g 1 22, o-1 <br />Notes: <br />1. EPA Method 8260B analyses must include all analytes listed in the method plus fuel oxygenates methyl - <br />tertiary -butyl ether (MTBE), diisopropyl ether (DIPE), ethyl -tertiary -butyl ether (EtBE), tertiary -amyl -methyl <br />ether (TAME), tertiary -butanol (TBA), methanol and ethanol and fuel additives 1,2-dichloroethane (1,2 -DCA) <br />and ethylene dibromide (EDB or 1,2-dibromoethane). <br />2. If pentachlorophenol (PCP) is identified, analyze the soil and/or water sample for dioxins and furans by EPA <br />Method 8290 and pesticides by EPA Method 8081A. <br />3. METALS ICAP or AA Inductively Coupled Plasma Atomic Emission Spectrometry 6010 or Atomic <br />Absorption Spectrometry 7000. Metals: Cadmium, Chromium III and VI, Lead, Zinc and Nickel. <br />4. Non-proprietary, performance based analytical methods may be used with approval of Regional Board staff. <br />EH 23 046 (Revised 8/3/07) <br />TANK <br />TANK <br />TPH-G <br />TPH-D <br />BTX & E <br />CL HC <br />TOTAL <br />MTBE <br />OXYGENATES <br />METALS <br />PCB <br /># <br />CONTENTS <br />LEAD <br />8270 <br />8015 <br />8015 <br />8020 <br />8010 <br />(MTBE ,TBA, DIPE, <br />ICAP/AES <br />8260 <br />8260 <br />8260 <br />8240 <br />7420 <br />8020 <br />ETRE, TAME) <br />or <br />8080 <br />8260 <br />7421 <br />8260 <br />1,2 DCA & EDB <br />AA <br />8260 <br />LEADED GAS <br />X <br />X <br />X <br />X <br />UNL GAS <br />X <br />X <br />X <br />DIESEL <br />X <br />X <br />KEROSENE <br />X <br />X <br />X <br />UNK FUEL <br />X <br />X <br />X <br />X <br />X <br />PROD. OIL <br />X <br />X <br />X <br />CHLOR. <br />SOLVENTS <br />X <br />X <br />X <br />NONCHLOR <br />SOLVENTS <br />X <br />X <br />X <br />WASTE\USED OIL <br />^ <br />./ ly <br />OR <br />UNKNOWN <br />X <br />X <br />X <br />X <br />j( <br />X <br />X <br />CONTENTS <br />g 1 22, o-1 <br />Notes: <br />1. EPA Method 8260B analyses must include all analytes listed in the method plus fuel oxygenates methyl - <br />tertiary -butyl ether (MTBE), diisopropyl ether (DIPE), ethyl -tertiary -butyl ether (EtBE), tertiary -amyl -methyl <br />ether (TAME), tertiary -butanol (TBA), methanol and ethanol and fuel additives 1,2-dichloroethane (1,2 -DCA) <br />and ethylene dibromide (EDB or 1,2-dibromoethane). <br />2. If pentachlorophenol (PCP) is identified, analyze the soil and/or water sample for dioxins and furans by EPA <br />Method 8290 and pesticides by EPA Method 8081A. <br />3. METALS ICAP or AA Inductively Coupled Plasma Atomic Emission Spectrometry 6010 or Atomic <br />Absorption Spectrometry 7000. Metals: Cadmium, Chromium III and VI, Lead, Zinc and Nickel. <br />4. Non-proprietary, performance based analytical methods may be used with approval of Regional Board staff. <br />EH 23 046 (Revised 8/3/07) <br />