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Iwpm laboratories 2905 Railroad Ave. Ceres, CA 95307 (209)581-9280 Fm(209)581-9292 <br />11 <br />11 <br />Ground Zero Analysis, Inc. <br />1172 Kansas Ave. <br />Modesto, CA 95351 <br />Argon Laboratories <br />Project Number: 952 <br />Project Name: Stockton RTD <br />Project Manager: Greg Stahl <br />Work Order No.: <br />P403002 <br />Reporting Spike Source %REC RPD <br />malyte Result Limit Units Level Result %d2EC Limits RPD Limit Notes <br />Approved By <br />' Argon Laboratories, Inc. California D.O.H.S. Cert. #2359 <br />I' Page 80 of 84 <br />Batch P111208 - EPA 50308 <br />'Batch <br />LCS Dup (P400208-BSDI) <br />Prepared & Analynd: 03/08/14 <br />Prepared & Analyzed: <br />03/09/14 <br />Chlorobenzene <br />0.074 mg/kg <br />0.025 95 <br />80-120 <br />5 <br />20 <br />Surrogate: Dilor m 7wromethane <br />1,1-Dichlomethene <br />0.028 <br />0.025 110 <br />80-120 <br />5 <br />20 <br />Surrogme: Toluene -d8 <br />Toluene <br />0.025 <br />11 <br />0.025 101 <br />80-120 <br />7 <br />20 <br />Surrogate: 4-EmmoJluorobemene <br />Trichloroethene <br />0.025 <br />0.025 101 <br />80-120 <br />3 <br />20 <br />Benzene <br />Matrix Spike (P400208 -MSI) <br />Source: P403002-15" <br />Prepared & Analyzed: 03/08/14 <br />' <br />Benzene <br />0.026 mg/kg <br />0.025 ND 105 <br />70.1 30 <br />'Bromobemene <br />Bromochloromethane <br />Chlorobenzene <br />0.023 <br />0.025 ND 94 <br />70-130 <br />Bromodichloromethene <br />1,1-Dichloroethene <br />0.028 <br />0.025 ND 111 <br />70-130 <br />'Toluene <br />ND <br />0.025 <br />0.025 ND 100 <br />70130 <br />Brumome0mne <br />Trichloroethene <br />0.025 <br />0.025 ND 98 <br />70130 <br />n -Butyl Benzene <br />Matrix Spike Dup (P40020&MSD1) <br />Source: P403002-15 <br />Prepared & Analyzed: 03/08/14 <br />sec -Butyl Benzene <br />ND <br />0.005 <br />" <br />-Butyl Benzene <br />Benzene <br />0.027 mg/kg <br />0.025 ND 109 <br />70130 <br />4 <br />20 <br />Carbon tetrachloride <br />Chlombeemme <br />0.024 <br />0.025 ND 97 <br />70130 <br />4 <br />20 <br />Chlorobenzene <br />10-Dichlomethme <br />0.027 <br />0.025 ND 107 <br />70130 <br />3 <br />20 <br />'Toluene <br />ND <br />0.026 I' <br />0.025 ND 105 <br />70130 <br />5 <br />20 <br />2-Chlomthylvinyl ether <br />Trichloroethene <br />0.026 <br />0.025 ND 102 <br />70-130 <br />4 <br />20 <br />Approved By <br />' Argon Laboratories, Inc. California D.O.H.S. Cert. #2359 <br />I' Page 80 of 84 <br />P400209 - EPA 5030B <br />'Batch <br />Prepared & Analyzed: <br />03/09/14 <br />Blank (P400209-BLKI) <br />Surrogate: Dilor m 7wromethane <br />0.0530 <br />mg/kg 0.050 <br />106 <br />70130 <br />Surrogme: Toluene -d8 <br />0.0565 <br />0.050 <br />113 <br />70130 <br />Surrogate: 4-EmmoJluorobemene <br />0.0505 <br />0.050 <br />101 <br />70130 <br />Benzene <br />ND <br />0.005 <br />" <br />ND <br />0.005 <br />'Bromobemene <br />Bromochloromethane <br />ND <br />0.005 <br />Bromodichloromethene <br />ND <br />0.005 <br />Brour four <br />ND <br />0.005 <br />" <br />Brumome0mne <br />ND <br />0.005 <br />n -Butyl Benzene <br />ND <br />0.005 <br />sec -Butyl Benzene <br />ND <br />0.005 <br />" <br />-Butyl Benzene <br />ND <br />0.005 <br />'t <br />Carbon tetrachloride <br />ND <br />0.005 <br />Chlorobenzene <br />ND <br />0.005 <br />Chloroethane <br />ND <br />0.005 <br />" <br />2-Chlomthylvinyl ether <br />ND <br />0.020 <br />" <br />Approved By <br />' Argon Laboratories, Inc. California D.O.H.S. Cert. #2359 <br />I' Page 80 of 84 <br />