Laserfiche WebLink
MINIMUM VERIFICATION LABORATORY ANALYSIS <br /> OXYGENAM <br /> aBTALS <br /> FTANKTANK TPHG TPH-D BTX & E CL HC TOTAL MTBE TBA,DtPE. ICAP/ 8270 <br /> PCB <br /> Y'TS 8(115 8015 8020 8010 LEAD 8020 ETRE. AES 8080 <br /> 8260 8260 8260 8240 7420 8260 TAME) or <br /> 8260 7421 8260 AA <br /> D GAS X X X X <br /> UNL GAS X X X <br /> DIESEL X X <br /> KEROSENE X X X <br /> UNK FUEL X X X X X <br /> PROD. OIL X X X <br /> CHLOR. X X X <br /> SOLVENTS <br /> NONCHL X <br /> SOLVENTS X X <br /> WASTEN X X <br /> f USED OIL X X X X X <br /> All analysis methods are the designated EPA methods described in EPA SW 846, Third Edition. Those methods not found in SW <br /> 846 are specifically noted below. Refer to the "SWRCB LUFT Field Manual". Appendix D(B),Table 3-5 on page A20 for <br /> minimum detection limits for motor vehicle fuel (gasoline and diesel). Refer to "Tri-Regional Board Staff Recommendations for <br /> Initial Evaluation and Investigation of UST's" for the waste and motor oil minimum detection limits. <br /> Detection Limits that remain below the MCL, STLC or Allowable Limit of the contaminant in question will be accepted, <br /> however laboratory shall utilize the most conservative method. <br /> LABORATORY ANALYSES TERMINOLOGY: <br /> TPH-G Total Petroleum Hydrocarbon, Gasoline, GC/FID(5030)8015 mud or GC/MS 8260 <br /> TPH-D Total Petroleum Hydrocarbon, Diesel, GC/FID(3550), 8015 mod or GC/MS 8260 <br /> 8TX& E Bemene, Toluene, Xylene&Ethyl Benzene, GC/PID 8020 or GC/MS 8260 <br /> CL HC Chlorinated Hydrocarbon, GC/HSD 8010, GC/MS 8240 or 8260 <br /> TOTAL LEAD Total lead, AA 7420, AA 7421 or ICP-AES 6010 <br /> OXYGENATES ' MTBE, ETRE,TAME, DIPE,&TBA GCIMS 8260(For MTBE screen only you may use 8020) <br /> METALS ICAP or AA Inductively Coupled Plasma Atomic Emission Spectrometry 6010 or Atomic Absorption Spectrometry 7000. <br /> Metals:Cadmium, Chromlum 111 and VI, Lead,Zinc and Nickel. <br /> PCB Polychlorinated Biphenyls,GC/MS 8270 or 8080 <br /> GC-FID Gas Chromatography, Flame loni2atiun Detection <br /> Method 3050 Acid digestion <br /> Method 3540 Soxhlet sample preparation <br /> Method 3550 Sonication sample preparation,extraction method <br /> Method 5030 Purge and trap sample preparation <br /> QA/QC Quality Assurance/Quality Control <br /> Notes: To avoid false positive detection of bem;oe, benzene-free solvents are to he used. Fused capillary columns are preferred to packed <br /> columns;a packed column may be used as a "first cut" with "dirty" samples or once the hydrocarbons have been characterized and proper <br /> QA/QC is followed. <br /> For drinking water xnrces, EPA recommends that the 500 series far volatile organic should be used in preference to the 600 series because the <br /> detection limits are lower and the QAIQC is better. Samples exhibiting any level of heavy metal contamination may require further analysis. <br /> PHS EHD recommends holding those samples until disposal is indicated. <br /> Eli 23 046 (Revised 05/09/00) Page 8 <br />