Laserfiche WebLink
1/182005 09:01 2094683 EHD • PAGE 06 <br /> MINIMUM VERIFICATION LA80RATORYANALY3IIXYGS <br /> TANK TANK TPH-G TPH-D BTX&E CL HC TOTAL MTBE RTES EN <br /> a CONTENTS 8015 8015 8020 afzrno PCB <br /> 8010 LPdaD 8020 (arfliE, ICAP/ 8270 <br /> 8260 8260 8260 8240 7420 8260 TBhDmE, <br /> 8260 7421 ETBL•, AES or 8080 <br /> TAMIL) AA <br /> 8260 <br /> LD•ADIED GAS X X <br /> x X <br /> UNL GAS X X <br /> X <br /> ].ESEL X X <br /> KEROSENE X X X <br /> INK FUEL X X X X <br /> X <br /> PROD.OIL X X X <br /> CHLOR. <br /> SOLVENTS X X X <br /> NONCHLOR <br /> SOLVENTS X X X <br /> WASTE\ <br /> USED OIL X X X X <br /> X X X <br /> A II analysis methods arc the designated EPA methods described In EPA SW 846,Third Edition. 'Those in not found hs$W.846 are <br /> specifi ally noted below, Refrr to the "SWRCB LUFT Field Manual",Appendix D (B),Table 3.5 on page A20 for minimum detection <br /> limits jor motor vehicle fuel (,esolint and diesel). Refer to "Tri-Rogional Board Staff Recommendations for Initial Evaluation and <br /> Investigation of US75" for the waste and motor oil minimum detection limits. Detection Limits tbat remain below the MCL,$TLC or <br /> Allowx Ic Limit or the contaminant in question will be accepted,however laboratory%ball utilize the most conservative method. <br /> LAHOI <br /> TPH-G Toil Petroleum Hydrocarbon, Gasoline,GC/FID)(50 0)6015 mod or GC/MTORYANALYSES S TERMINOLOGY: <br /> TnI-D Total Pcuoleum Hydrocarbon,Diesel,GGFID(3550),8015 mod or GC/MS 8260 <br /> BTX& Beruene,TOlUenc,Xylcne&Ethyl Benzcne,GC/PM 8020 or GUMS 9260 <br /> CL HC Chlorinated Ilydroearbon,GC/HSD 8010,GC/MS R24D or 8260 <br /> TOTAL- EAD l'otal lead,AA 1420, AA 7421 or ICP-AES 6010 <br /> OXYGE ATES MTBE,ETBE,TAME,D1PE,&TBA GC/MS 6260(For MTBE r n you may use 6020) <br /> MET ICAP ur AA Inductively Coupled Plasmo Atonic Emission Spectrometry 6010 or Atomic Absorption Spectrometry 7000. Mctals: <br /> Cadmium,Chromium 111 and VI,.Lead,Zine and Nickel. <br /> PCB Polychlorinatcd Biphenyls,GCIMS 8170 or 8080 <br /> GC-FID Gas CMomatogrephy,FIame Ionization Detection <br /> Method 3050 Acid digestion <br /> Method 3540 Soxhlct sample preparation <br /> Method 3550 Sonicaion sample prepanxion,extraction method <br /> Method 3030 Purge told trap sample preparation <br /> QA/QC Quality Assurunce/Qu lity Control <br /> Notes: Tt avoid false positive detection of benzene,benzene-frac solvents arc to be used. Fused capillmy columns ore preferred to packed columns,a <br /> packed co mmn may be used m a "first cut"with"dirty"samples or once the hydrocarbons have been ehsractorizcd and proper QA/QC is followed. For <br /> drinking v o'er sanr:es,EPA rccommatds that the 500 series for voludle organic should be used in preference to the 600 series because the detection <br /> lim60 are war and the QA/QC is better. Samples exhibiting any level of heavy metal contaminotion may require further anolysis.PHS-EHD <br /> r=Omncn Is holding those samples until disyasal is indicated. <br /> EH 23 046 (Reviled 051091oo) <br /> 5 <br />