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Page 13 of 24 <br /> alscience <br /> nvironmental Quality Control - Spike/Spike Duplicate <br /> aboratories, Inc. <br /> Kiff Analytical Date Received: 12/06/08 <br /> 2795 2nd Street, Suite 300 Work Order No: 08-12-0742 <br /> Davis, CA 95616-6593 Preparation: EPA 3545 <br /> Method: EPA 8270C <br /> Proiect Edison St. <br /> Date Date MS/MSD Batch <br /> Quality Control Sample ID Matrix Instrument Prepared Analyzed Number <br /> 08-12-0361-17 Solid GUMS SS 12/08/08 12/09/08 081208S09 <br /> Parameter MS%REC MSD%REC %REC CL RPD RPD CL Qualifiers <br /> Phenol 83 72 57-123 14 0-16 <br /> 2-Chlorophenol 80 70 57-111 14 0-17 <br /> 1,4-Dichlorobenzene 93 81 49-127 14 0-20 <br /> N-Nitroso-di-n-propylamine 97 85 54-144 14 0-17 <br /> 1,2,4-Trichlorobenzene 89 80 42-132 11 0-20 <br /> Naphthalene 94 83 50-150 12 0-20 <br /> 4-Chloro-3-Methyl phenol 92 82 50-128 11 0-17 <br /> Dimethyl Phthalate 83 74 50-150 12 0-20 <br /> Acenaphthylene 93 83 50-150 11 0-20 <br /> Acenaphthene 92 83 49-133 10 0-18 <br /> 4-Nitrophenol 95 81 30-144 16 0-21 <br /> 2,4-Dinitrotoluene 86 74 50-128 14 0-18 <br /> Fluorene 101 91 50-150 10 0-20 <br /> Pentachlorophenol 65 59 29-113 10 0-22 <br /> Pyrene 89 83 47-149 7 0-20 <br /> Butyl Benzyl Phthalate 88 81 50-150 8 0-20 <br /> RPD-Relative Percent Difference, CL-Control Limit <br /> 7440 Lincoln Way, Garden Grove, CA 92841-1427 . TEL:(714) 895-5494 FAX: (714) 894-7501 <br />