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Page 14 of 22 <br /> alscience <br /> nvironmental Quality Control - Spike/Spike Duplicate <br /> aboratories, Inc. <br /> Kiff Analytical Date Received: 01/17/09 <br /> 2795 2nd Street, Suite 300 Work Order No: 09-01-1418 <br /> Davis, CA 95616-6593 Preparation: EPA 3545 <br /> Method: EPA 8270C <br /> Proiect Stockton Promenade <br /> Date Date MS/MSD Batch <br /> Quality Control Sample ID Matrix Instrument Prepared Analyzed Number <br /> 09-01-1393-2 Solid GUMS SS 01/19/09 01/21/09 090119S11 <br /> Parameter MS%REC MSD%REC %REC CL RPD RPD CL Qualifiers <br /> Phenol 92 108 57-123 16 0-16 <br /> 2-Chlorophenol 89 103 57-111 15 0-17 <br /> 1,4-Dichlorobenzene 85 97 49-127 12 0-20 <br /> N-Nitroso-di-n-propylamine 104 120 54-144 15 0-17 <br /> 1,2,4-Trichlorobenzene 81 92 42-132 13 0-20 <br /> Naphthalene 85 96 50-150 13 0-20 <br /> 4-Chloro-3-Methyl phenol 86 99 50-128 14 0-17 <br /> Dimethyl Phthalate 81 92 50-150 13 0-20 <br /> Acenaphthylene 85 96 50-150 12 0-20 <br /> Acenaphthene 85 95 49-133 11 0-18 <br /> 4-Nitrophenol 97 111 30-144 14 0-21 <br /> 2,4-Dinitrotoluene 91 105 50-128 15 0-18 <br /> Fluorene 88 100 50-150 12 0-20 <br /> Pentachlorophenol 82 96 29-113 16 0-22 <br /> Pyrene 87 99 47-149 13 0-20 <br /> Butyl Benzyl Phthalate 91 102 50-150 11 0-20 <br /> RPD-Relative Percent Difference, CL-Control Limit <br /> 7440 Lincoln Way, Garden Grove, CA 92841-1427 . TEL:(714) 895-5494 FAX: (714) 894-7501 <br />