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110 Second Avenue South,#D7,Pacheco,CA 94553 <br /> MCCAMPBELL ANALYTICAL INC. Telephone:510-798-1620 Fax:510-798-1622 <br /> 14 http://wAw.mccamr)bell.com E-mail:main@mccampbelI.com <br /> Advanced GeoEnvirortmentai Client Project ID: Certified Grocery Date Sampled: 09125-09/26/97 <br /> 1803 West March Lane, Ste A Date Received: 09/30/97 <br /> Stockton, CA 95207 Client Contact:Bill Little Date Extracted: 09/30/97 <br /> Client P.O: Date Analyzed: 09/30-10/01/97 <br /> Diesel Range(C10-C23)Extractable Hydrocarbons as Diesel <br /> EPA methods modified 8015,and 3550 or 3510;California RWQCB(SF Say Region)method GCF1D(3550)or GCFID(3510) <br /> Lab ID Client ID Matrix TPH(d)+ %Recovery <br /> Surrogate <br /> 81289 SP1 S 1.6,b 106 <br /> 81290 SP2 S 130,c 108 <br /> 81291 SP3 S 60,c 93 <br /> 81292 SP4 S 79,a 93 <br /> 81293 SP5 S 190,a 93 <br /> 81294 SPG S 27•a 93 <br /> 81295 SP7 S 760,g,b 107 <br /> 81296 SP8 S 5200,a 96 <br /> 81297 TS-1 S ND 106 <br /> 81298 TS-2 S ND 106 <br /> 81299 TS-3 S ND 106 <br /> Reporting Limit unless otherwise W 50 ug/L <br /> stated;ND means not detected above <br /> the reporting limit S LO mg/kg <br /> *water and vapor samples are reported in ug/L.,wipe samples in ug/wipe,soil and sludge samples in mg/kg,and all TCLP/STLC/SPLP <br /> extracts in ug/L <br /> "cluttered chromatogram resulting in coeluted surrogate and sample peaks,or;surrogate peak is on elevated baseline,or;surrogate has been <br /> diminished by dilution of original extract. <br /> 'The following descriptions of the TPH chromatogram are cursory in nature and McCampbell Analytical is not responsible for their <br /> interpretation:a)unmodified or weakly modified diesel is significant;b)diesel range compounds are significant;no recognizable pattern;c) <br /> aged diesel?is significant);d)gasoline range compounds are significant;e)medium boiling point pattern that does not match diesel (?); f) <br /> one to a few isolated peaks present; g)oil range compounds are significant; h) lighter than water immiscible sheen is present; i) liquid <br /> sample that contains greater than—5 vol.%sediment. <br /> DHS Certification No. 1644 /�� Edward Hamilton,Lab Director <br />