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i./ -�•.� <br /> 110 Second Avenue South,##D7,Pacheco,CA 94553 <br /> MCCAMPBELL ANALYTICAL INC. Telephone: 510-798-1620 Fax: 510-798-1622 <br /> 24 http://www.mcE2M2bell.com E-mail:main@mccampbell.com <br /> Date Sampled: 10/01/97 <br /> Advanced GeoEnvironmental Client Project ID:Certified Grocery <br /> Date Received: 10/02/97 <br /> 1803 West March Lane,Ste A <br /> Stockton, CA 95207 Client Contact:Bill Little Date Extracted: 10/02/97 <br /> Client P.O: Date Analyzed: 10/02-10/03/97 <br /> Diesel Range(C10-C23) and Oil-Range(C18+)Extractable Hydrocarbons as Diesel and Motor Oil* <br /> EPA methods modified 8015,and 3550 or 3510;California RWQCB(SF Bay Region)method GCF1D(3550)or GCFID(3510) <br /> Lab ID Client ID Matrix TPH(d)+ TPH(mo)' %Recovery <br /> Surrogate <br /> 81463 P-1 S ND --- 107 <br /> 81464 P-2 S ND --- 93 <br /> 81465 P-3 S 33,g --- 92 <br /> 81466 P-4 S ND --- 101 <br /> 81467 P-5 S ND ND 105 <br /> 81468 P-6 S 21,g,b 84 112 <br /> 81469 P-7 S 780,8 3800 93 <br /> 81470 D1 S 21,b,g --- 109 <br /> 81471 1 A S N D --- 106 <br /> 81472 2A S 2800,g,b --- 101 <br /> Reporting Limit unless otherwise W 50 ug/L 250 ug/L <br /> stated;ND means not detected above <br /> the reporting limit S 1.0 mg/kg 5.0 mg/kg <br /> *water samples are reported in ug/L,wipe samples in ug/wipe,soil and sludge samples in mg/kg,and all TCLP I STLC I SPLP extracts in <br /> ug/L <br /> 0 cluttered chromatogram resulting in coeluted surrogate and sample peaks,Or;surrogate peak is on elevated baseline,or;surrogate has been <br /> diminished by dilution of original extract. <br /> 'The following descriptions of the TPH chromatogram are cursory in nature and McCampbell Analytical is not responsible for their <br /> interpretation:a)unmodified or weakly modified diesel is significant;b)diesel range compounds are significant;no recognizable pattern;e) <br /> aged diesel?is significant);d)gasoline range compounds are significant;e)medium boiling point pattern that does not match diesel(?); f) <br /> one to a few isolated peaks present; g)oil range compounds are significant; h) lighter than water immiscible sheen is present; i) liquid <br /> sample that contains greater than--5 vol.%sediment. <br /> DHS Certification No. 1644 /!2 Edward Hamilton,Lab Director <br />