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FRIEDMAN &BRUYA, INC. <br /> ENVIRONMENTAL CHEMISTS <br /> Analysis For PNA Compounds By EPA Method 8270C SIM <br /> Client Sample ID: D119-14.5-15 Client: Earth Systeme Consultants <br /> Date Received: 08/03/99 Project: NFE-4533-01 <br /> Date Extracted: 08/04/99 Lab ID: 908010.02 1/10 <br /> Date Analyzed: 08/05/99 Data File: 080420.1) <br /> Matrix: Soil Instrument: GCMS#2 <br /> Units: ug/kg(ppb) Operator: YA <br /> Lower Upper <br /> Surrogates: %Recovery Limit Limit <br /> Anthracene-d10 92 50 150 <br /> Benzo(a)anthracene-d12 122 50 150 <br /> Concentration <br /> Compounds: ug/kg(ppb) <br /> Naphthalene <50 <br /> Acenaphthylene <50 <br /> Acenaphthene 160 <br /> Fluorene 490 <br /> Phenanthrene 720 <br /> Anthracene <50 <br /> Fluormthene <50 <br /> Pyrene 93 <br /> Benz(a)anthracene <50 <br /> Chrysene 140 <br /> Benzo(b)fluormthene <50 <br /> Benzo(k)fluoranthene <50 <br /> Benzo(a)pyrene <50 <br /> Indeno(1,2,3-cd)pyrene <50 <br /> Dibenzo(a,h)anthracene <50 <br /> Benzo(g,h,i)perylene <50 <br /> Note: The sample was diluted due to the presence of high levels of material. Detection limits are raised <br /> due to dilution and surrogate recoveries may not be meaningful. <br /> 4 <br />