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FRIEDMM& BRUYA, INC. <br /> ENVIRONMENTAL CHEMISTS <br /> Analysis For Volatile Compounds By EPA Method 8260B <br /> Client Sample ID: GMX-6-11.5 Client: Geomatrix Consultants, Inc. <br /> Date Received: 09/24/99 Project: 5650 <br /> Date Extracted: 09/24/99 Lab ID: 909106-06 <br /> Date Analyzed: 09/24/99 Data File: 092416.D <br /> Matrix: Soil Instrument: GCMSI <br /> Units: ug/kg (ppb) Operator: YA <br /> Lower Upper <br /> Surrogates: %Recovery Limit Limit <br /> Dibromofluoromethane 91 50 150 <br /> 1,2-Dichloroethane-d4 97 50 150 <br /> Toluene-d8 255ip 50 150 <br /> 4-Bromofluorobenzene 397 ip 50 150 <br /> Concentration <br /> Compounds: ug/kg(ppb) - <br /> Methyl t-butyl ether(MTBE) <5 <br /> Benzene <5 <br /> Toluene <5 <br /> Ethylbenzene <5 <br /> m,p-Xylene <5 <br /> o-Xylene <5 <br /> ip -Recovery fell outside of normal control limits. Compounds in the sample matrix interfered with the <br /> quantitation of the analyte. <br /> 8 <br />