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FRIEDMAN& BRUYA, INC. <br /> ENVIRONMENTAL CHEMISTS <br /> Analysis For Volatile Compounds By EPA Method 8260B <br /> Client Sample ID: GMX-13-12.5 Client: Geomatrix Consultants, Inc. <br /> Date Received: 09/27/99 Project: 5650 <br /> Date Extracted: 09/27/99 Lab ID: 909112-03 <br /> Date Analyzed: 09/28/99 - Data File: 09281 LD <br /> Matrix: Soil Instrument: GCMS1 <br /> Units: ug/kg (ppb) Operator: YA <br /> Lower Upper <br /> Surrogates: %Recovery Limit Limit <br /> Dibromofluoromethane 92 50 150 <br /> 1,2.Dichloroethane-d4 102 50 150 <br /> Toluene-d8 163 ip 50 150 <br /> 4-Bromofluorobenzene 127 50 150 <br /> Concentration <br /> Compounds: ug/kg(ppb) <br /> Methyl t-butyl ether (MTBE) <50 <br /> Benzene <50 <br /> Toluene <50 <br /> Ethylbenzene 1,300 <br /> m,p-Xylene 550 <br /> o-Xylene <50 <br /> Note: The sample was diluted due to high levels of interfering compounds. Detection limits are raised <br /> due to dilution. <br /> ip - Recovery fell outside of normal control limits. Compounds in the sample matrix interfered with the <br /> quantitation of the analyte. <br /> 3 <br />