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FREEDMAN & BRUYA, INC. <br /> ENVIRONMENTAL CHEMISTS <br /> Date of Report: 06/07/00 <br /> Date Received: 05/17/00 <br /> Project: 6115.008 <br /> QUALITY ASSURANCE RESULTS FOR THE ANALYSIS OF SOIL SAMPLES <br /> FOR PNA'S BY EPA METHOD 8270C SIM <br /> Laboratory Code:-005091-04- (Duplicate) <br /> Reporting Sample Duplicate Acceptance <br /> Analvte Units Result Result RPD Criteria <br /> Napthalene pg/kg(ppb) <5 <5 nm 0-20 <br /> Acenapthylene pg/kg(ppb) <5 <5 nm 0-20 <br /> Acenapthene pg/kg(ppb) ' <5 <5 nm 0-20 <br /> Fluorene pg/kg (ppb) <5 <5 nm 0-20 <br /> Phenanthrene pg/kg (ppb) <5 <5 nm 0-20 <br /> Anthracene pg/kg(ppb) <5 <5 nm 0-20 <br /> Fluoranthene pg/kg(ppb) <5 <5 nm 0-20 <br /> Pyrene pg/kg(ppb) <5 <5 nm 0-20 <br /> Benz(a)anthracene pg/kg (ppb) <5 <5 nm 0.20 <br /> Chrysene pg/kg(ppb) <5 <5 nm 0-20 <br /> Benzo(b)fluoranthene pg/kg(ppb) <5 <5 nm 0-20 <br /> Benzo(k)fluoranthene pg/kg(ppb) <5 <5 nm 0-20 <br /> Benw(a)pyrene pg/kg(ppb) <5 <5 nm 0-20 <br /> Indeno(1,2,3-cd)pyrene gg/kg(ppb) <5 <5 nm 0.20 <br /> Dibenzo(a,h)anthracene pg/kg(ppb) <5 <5 nm 0-20 <br /> Benw(g,h,i)perylene nikg(ppb) <5 <5 nm 0-20 <br /> Laboratory Code: 005091.04 (Matrix Spike) <br /> Reporting Spike Sample %Recovery %Recovery Acceptance <br /> Anaivte Units Level Result MS MSD Criteria RPD <br /> Napthalene µg/kg(ppb) 170 <5 70 73 56.117 5 <br /> Acem pthylene pg/kg(ppb) 170 <5 73 78 59-115 6 <br /> Acenapthene pg/kg(ppb) 170 <5 72 77 59-114 7 <br /> Fluorene pg/kg(ppb) 170 <5 70 75 61-113 7 <br /> Phenanthrene pg/kg (ppb) 170 <5 68 72 51-122 5 <br /> Anthracene pg/kg(ppb) 170 <5 72 76 50-116 5 <br /> Fluoranthene pg/kg (ppb) 170 <5 78 80 52-124 4 <br /> Pyrene pg/kg (ppb) 170 <5 76 81 49-124 7 <br /> Benz(a)anthracene pg/kg(ppb) 170 <5 66 72 50-122 8 <br /> Chrysene gg/kg(ppb) 170 <5 71 77 48-121 7 <br /> Benw(b)fluoranthene n/kg(ppb) 170 <5 69 68 52-144 1 <br /> Benw(k)fluoranthene µg/kg(ppb) 170 <5 70 78 55-135 11 <br /> Benzo(a)pyrene n/kg(ppb) 170 <5 66 69 49-128 4 <br /> Indeno(1,23-cd)pyrene µg/kg (ppb) 170 <5 82 87 36-132 6 <br /> Dibenw(a,h)anthracene µg/kg(ppb) 170 <5 81 85 37.136 5 <br /> Benzo(g,h,i)perylene pg/kg (ppb) 170 <5 79 83 28.132 5 <br /> nm - The analyte was not detected in one or more of the duplicate analyses. Therefore, calculation of <br /> the RPD is not applicable. <br /> 24 <br />