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07/03/2007 09:06 FAX 4084515050 CLEAN HARBORS ENV. SRV. 121004/021 <br /> Excelchem Environmental Labs <br /> CLS Environmental Project: Flying J-Ripon <br /> 8 Crow Canyon Rd,Suite 205 Project Number: FJI-117 Date Reported: <br /> San Ramon.CA 94583 Project Manager: Travis Springer 12/06/06 16:30 <br /> OWS-1 <br /> 0611079-01 (Water) <br /> Reporting Date Date <br /> Analyte Result Limit Units Batch Prepared Analyzed Method Notes <br /> METALS'BY 6000/7000 SERIES <br /> Antimony 20.6 10.0 ug/1 APK0139 11/22/06 11/22/06 EPA 6010B <br /> Arsenic 39.6 10.0 11/22/06 " <br /> Barium 303 20.0 11/22/06 " <br /> Beryllium ND 5.0 " <br /> Cadmium 63.5 10.0 11/22/06 <br /> Chromium 42.7 10.0 " <br /> Cobalt ND 50.0 " <br /> Copper 814 20.0 11/22/06 " <br /> Lead 76.6 10.0 " <br /> Mercury <br /> ND 0.250 APK0140 11/22/06 11/22/06 EPA 7470A <br /> Molybdenum 16.1 10.0 APK0139 11/22/06 11/22/06 EPA 6010B <br /> Nickel 24.1 10.0 " <br /> Selenium 46.6 20.0 " <br /> Silver 22.2 20.0 11/22/06 " <br /> Thallium ND 20.0 " <br /> Vanadium 36.0 20.0 " <br /> Zinc 529 20.0 11/22/06 " <br /> Volatile Organic Compounds by GC/MS <br /> Gasoline Range Hydrocarbons 9820 5000 ug/I APK0116 11/20/06 11/21/06 EPA 8260B D-02 <br /> TBA ND 500 <br /> Methyl tert-Butyl Ether ND 50.0 " <br /> Di-isopropyl ether ND 50.0 ; <br /> Ethyl tert-Butyl Ether ND 50.0 " <br /> Tert-Amyl Methyl Ether ND 50.0 " <br /> Dichlorodifluoromethane ND 50.0 " <br /> Chloromethane ND 50.0 " <br /> Vinyl chloride ND 50.0 <br /> Bromomethane ND 50.0 " <br /> Chloroethane ND 50.0 " <br /> Trichlorofluoromethane ND 50.0 " <br /> Acetone ND 1000 " <br /> 1,1-Dichloroethene ND 50.0 <br /> lodomeihane ND 50.0 " <br /> Methylene chloride ND 100 <br /> Carbon disulfide ND 50.0 " <br /> trans-1,2-Dichloroethene ND 50.0 " <br /> EXcelchem Environmental Lab The results in this report apply to the samples analyzed in accordance with the chain of <br /> custody document. This analytical report must be reproduced in its entirety. <br /> Laboratory Representative Page 2 of 18 <br />