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07/03/2007 09:09 FAX 4084515050 CLEAN HARBORS ENV. SRV. IdI 011/021 <br /> Excelchem Environmental Labs <br /> CLS Environmental Project: Flying J-Ripon <br /> 8 Crow Canyon Rd,Suite 205 Project Number: FJI-117 Date Reported: <br /> San Ramon,CA 94583 Project Manager: Travis Springer 12/06/06 16:30 <br /> METALS BY 6000/7000 SERIES- Quality Control <br /> Repprting S tke gource °//oC Mi <br /> Analyte Result LiAU Units Level Result %REC Limits RPD t Nows <br /> Batch APK0139 - EPA 6010B _ <br /> Matrix Spike Dup(APK0139-MSD1)_ Source_:0611079-01 Prepared&Analyzed: 11/22/06 <br /> Antimony 939 10.0 ug/l 1000 20.6 91.8 75-125 9.24 25 <br /> Arsenic 1000 10.0 1000 39.6 96.0 75-125 8.61 25 <br /> Barium 1200 20.0 1000 303 89.7 75-125 3.28 25 <br /> Beryllium 998 5.0 1000 0.4 99.8 75-125 3.78 25 <br /> Cadmium 938 10.0 1000 63.5 87.4 75-125 4.28 25 <br /> Chromium 962 10.0 1000 42.7 91.9 75-125 1.04 25 <br /> Cobalt 902 50.0 1000 12.7 88.9 75-125 17.6 25 <br /> Copper 1370 20.0 1000 814 55.6 75-125 14.9 25 QM-07 <br /> Lead 892 10.0 1000 76.6 81.5 75-125 14.4 25 <br /> Molybdenum 942 10.0 1000 16.1 92.6 75-125 19.7 25 <br /> Nickel 874 10.0 1000 24.1 85.0 75-125 27.5 25 QR-03 <br /> Selenium 862 20.0 1000 46.6 81.5 75-125 21.5 25 <br /> Silver 789 20.0 1000 22.2 76.7 75-125 11.7 25 <br /> Thallium 766 20.0 1000 ND 76.6 75-125 14.6 25 <br /> Vanadium 837 20.0 1000 36.0 80.1 75-125 14.1 25 <br /> Zinc 926 20.0 1000 529 39.7 75-125 0.00 25 QM-07 <br /> Batch APK0140-EPA 7470A <br /> Blank(APK0140-BLKI)_ _ Prepared&Analyzed: 11/22/06 <br /> Mercury ND 0.250 ug/l <br /> LCS(APK0140-BSI) _ Prepared&Analyzed: 11/22/06 <br /> Mercury. 5.26 0.250 ug/1 5.00 1 G 5 80-120 <br /> LCS Du p(APK0140-BSD1 - Prepared&Analyzed: 11/22/06 <br /> Mercury 5.28 0.250 ug/l 5.00 106 80-120 0.380 20 <br /> Excelchem Environmental Lab. The results in this report apply to the samples analyzed in accordance with the chain of. <br /> custody document. This analytical report must be reproduced in its entirety. <br /> Laboratory Representative Page of 18 <br />