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07/03/2007 09: 10 FAX 4084515050 CLEAN HARBORS ENV. SRV. 0013/021 Excelchem Environmental Labs CLS Environmental Project: Flying J-Ripon 8 Crow Canyon Rd,Suite 205 Project Number: FJI-117 Date Reported: San Ramon,CA 94583 Project Manager: Travis Springer 12/06/06 16:30 Volatile Organic Compounds by GC/MS- Quality Control Re QQrain ptk W,,,,Ie °61C A Analyte Result Rep Units eve esuclt %REC tmIts RPD tmtt Notes Batch APKO116-EPA 8260B Blank(APK0116-BLKI) Prepared: 11/20/06 Analyzed: 11/21/06 Surrogate:Dibromofluoromethane 11.9 ug/l 12.5 95.2 70-130 Surrogate:Toluene-d8 12.2 12.5 97.6 70-130 Surrogate:4-Bromgfluoroben_ene 12.1 12.5 96.8 70-130 Dichlorodifluoromethane ND 0.5 " Chloromethane ND 0.5 " Vinyl chloride ND 0.5 " Bromomethane ND 0.5 " Chloroethane ND 0.5 " Trichlorofluoromethane ND 0.5 " Acetone ND 10.0 " 1,1-Dichloroethene ND 0.5 " lodomethane ND 0.5 " Methylene chloride ND 1.0 " Carbon disulfide ND 0.5 " trans-1,2-Dichloroethene ND 0.5 " 1.1-Dichloroethane ND 0.5 2-Butanone ND 5.0 " 2,2-Dichloropropane ND 0.5 " cis-1,2-Dichloroethene ND 0.5 " Bromochloromethane ND 0.5 " Chloroform ND 0.5 " 1,1,1-Trichloroethane ND 0.5 " Carbon tetrachloride ND 0.5 " 1,1-Dichloropropene ND 0.5 " Benzene ND 0.5 " 1,2-Dichloroethane ND 0.5 ' Trichloroethene ND 0.5 " 1,2-Dichloropropane ND 0.5 " Dibromomethane ND 0.5 " Bromodichloromethane ND 0.5 " cis-1,3-Dichloropropene ND 0.5 " 4-Methyl-2-pentanone ND 5.0 " Toluene ND 0.5 " trans-1,3-Dichloropropene ND 0.5 1,1,2-Trichloroethane ND 0.5 " Tetrachloroethene ND 0.5 1,3-Dichloropropane ND 0.5 " 2-Hexanone ND 5.0 " Dibromochloromethane ND 0.5 " Excelchem Environmental Lab. The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. Laboratory Representative Page I I o£18