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07/03/2007 09:11 FAX 4084515050 CLEAN HARBORS ENV. SRV, 10017/021 Excelchem Environmental Labs CLS Environmental Project: Flying J-Ripon 8 Crow Canyon Rd,Suite 205 Project Number: FJI-117 Date Reported: San Ramon,CA 94583 Project Manager: Travis Springer 12/06/06 16:30 SemiVolatile Organic Compounds by GC/MS- Quality Control Re rain gptk gourCe o °//oR1~C L? Analyte Result Rep Units Levees Result /oREC Lt E RPD tmtt Notes Batch APK0119-EPA 8270C Blank(APK0119-BLKI) Prepared&Analyzed: 11/21/06 Surrogate:2-Fluorophenol 21.4 mg/L 50.0 42.8 10-110 Surrogate:Phenol-d6 14.2 50.0 28.4 10-110 Surrogate:Nitrobenzene-d5 27.3 50.0 54.6 10-110 Surrogate:2-Fluorobiphenyl 26.8 50.0 53.6 10-110 Surrogate:2,4,6-Tribromophenol 36.4 50.0 72.8 10-110 Surrogate: Terphenyl-dN 36.6 50.0 73.1 10-110 N-Nitrosodimethylamine ND 2.0 ug/I Aniline ND 2.0 " Bis(2-chloroethyl)ether ND 2.0 Phenol ND 2.0 " 2-Chlorophenol ND 2.0 " 1,4-Dichlorobenzene ND 2.0 " Benzyl alcohol ND 2.0 " Bis(2-chloroisopropyDether 16 2.0 " 2-Methylphenol ND 2.0 " Hexachloroethane ND 2.0 " N-Nitrosodi-n-propylamine ND 2.0 " 4-Methylphenol ND 2.0 " Nitrobenzene ND 2.0 " Isophorone ND 2.0 " 2-Nitrophenol ND 2.0 " 2,4-Dimethylphenol ND 2.0 " Bis(2-chloroethoxy)methane ND 2.0 " Benzoic acid ND 10.0 " 2,4-Dichlorophenol ND 2.0 " 1,2,4-Trichlorobenzene ND 2.0 " Naphthalene ND 2.0 " 4-Chloroaniline ND 2.0 " Hexachlorobutadiene ND 2.0 " 4-Chloro-3-methylphenol ND 2.0 " 2-Methylnaphthalene ND 2.0 " Hexachlorocyclopentadiene ND 2.0 " 2,4,6-Trichlorophenol ND 2.0 " 2,4,5-Trichlorophenol ND 2.0 " 2-Chloronaphthalene ND 2.0 " 2-Nitroaniline ND 2.0 " Acenaphthylene ND 2.0 " Dimethyl phthalate ND 2.0 " 2.6-Dinitrotoluene ND 2.0 " Excelchem Environmental Lab. The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical?eport must be reproduced in its entirety. Laboratory Representative Page 15 of 18