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07/03/2007 11:53 FAX 4084515050 CLEAN HARBORS ENV. SRV. IA 006/021 <br /> Excelchem Environmental Labs <br /> CLS Environmental Project: Flying J-Ripon <br /> 8 Crow Canyon Rd,Suite 205 Project Number: FJI-117 Date Reported: <br /> San Ramon,CA 94583 Project Manager: Travis Springer 12/06/06 16:30 <br /> OWS-1 <br /> 0611079-01 (Water) <br /> Reporting Date Date <br /> Analvte Result Limit Units Batch Prepared Analyzed, Method Notes <br /> Volatile Organic Compounds by GC/MS <br /> 4-Chlorotoluene ND 50.0 ug/1 APK0116 11/20/06 11/21/06 EPA 52608 <br /> 1,3,5-Trimethylbenzene 62.0 50.0 " <br /> tert-Butylbenzene ND 50.0 <br /> 1,2,4-Trimethylbenzene 294 50.0 " <br /> sec-Butylbenzene ND 50.0 <br /> 1,3-Dichlorobenzene ND 50.0 " <br /> 4-Isopropyltoluene ND 50.0 <br /> 1,4-Dichlorobenzene ND 50.0 <br /> 1,2-Dichlorobenzene ND 50.0 <br /> n-Butylbenzene ND 50.0 " <br /> 1,2-Dibromo-3-chloropropane ND 50.0 " <br /> 1,2,4-Trichlorobenzene ND 50.0 " <br /> Hexachlorobutadiene ND 50.0 <br /> Naphthalene ND 50.0 " <br /> 1,2,3-Trichlorobenzene ND 50.0 <br /> Surrogate:Dibromofluoromethane 92.8% /o Recovery Limits 70-130 <br /> Surrogate: Toluene-d8 97.6% %Recovery Limits 70-130 <br /> Surrogate:4-Bromofluoroben_ene 93.6% %Recovery Limits 70-130 <br /> Total Petroleum Hydrocarbons by FID <br /> TPH as Diesel 2.64E7 400000 ug/1 APKOi 10 11/17/06 11/18/06 EPA 8015Mod <br /> TPH as Motor Oil ND 4000000 R-05 <br /> SemiVolatile Organic Compounds by GC/MS R-05 <br /> N-Nitrosodimethylamine ND 2400 ug/1 APKO119 11/20/06 11/21/06 EPA 8270C <br /> Aniline ND 2400 <br /> Bis(2-chloroethyl)ether ND 2400 <br /> Phenol ND 2400 <br /> 2-Chlorophenol NA 2400 <br /> 1.4-Dichlorobenzene ND 2400 <br /> Benzyl alcohol ND 2400 <br /> Bis(2-chloroisopropyl)ether ND 2400 <br /> 2-Methylphenol NID 2400 <br /> Hexachloroethane ND 2400 " <br /> N-Nitrosodi-n-propylamine ND 2400 <br /> 4-Methylphenol ND 2400 , <br /> Nitrobenzene ND 2400 <br /> Isophorone NL]l 2400 <br /> Excelchem Environmental Lai. The results in this report apply to the samples analyzed in accordance with the chain of <br /> custody document. This ana:ytical report must be reproduced in its entirety. <br /> Laboratory Representative Page 4 of 18 ' <br />