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07/03/2007 11:54 FAX 4084515050 CLEAN HARBORS ENV. SRV. 0 008/021 <br /> Excelchem Environmental Labs <br /> CLS Environmental Project: Flying J-Ripon <br /> 8 Crow Canyon Rd Suite 205 Project Number: FJI-117 Date Reported: <br /> San Ramon,CA 94583 Project Manager: Travis Springer 12/06/06 16:30 <br /> OWS-1 <br /> 0611079-01 (Water) <br /> Reporting Date Date <br /> Analyte Result Limit Units Batch Prepared Analyzed Method Notes <br /> SemiVolatile Organic Compounds by GUMS R-OS <br /> Di-n-butyl phthalate ND 2400 ug/l APK0119 11/20/06 11/21/06 EPA 8270C <br /> Fluoranthene ND 2400 " <br /> Benzidine ND 2400 <br /> Pyrene ND 2400 " <br /> Butyl benzyl phthalate ND 2400 " <br /> 3,3'-Dichlorobenzidine ND 2400 " <br /> Benzo(a)anthracene NO 2400 <br /> Chrysene ND 2400 " <br /> Bis(2-ethylhexyl)phthalate ND 2400 <br /> Di-n-octyl phthalate ND 2400 <br /> Benzo(b)fluoranthene ND 2400 " <br /> Benzo(k)fluoranthene ND 2400 " <br /> Benzo(a)pyrene ND 2400 " <br /> Indeno(1,2,3-cd)pyrene ND 2400 " <br /> Dibenz(ah)anthracene ND 2400 " <br /> Benzo(g,h,i)perylene ND 2400 _ <br /> Surrogate:2-Fluorophenol % %Recovery Limits 10-110 S-06 <br /> Surrogate:Phenol-d6 % %Recovery Limits 10-110 S-06 <br /> Surrogate:Nitrobenzene-d5 % %Recovery Limits 10-110 S-06 <br /> Surrogate:2-Fluorobiphenyl % %Recovery Limits 10-110 S-06 <br /> Surrogate:2,4,6-Tribromophenol % %Recovery Limits 10-110 S-06 <br /> Surrogate:Terphenyl-dN % %Recovery Limits 10-110 S-06 <br /> EXcelchem Environmental Lab. The results in this report apply to the satnples analyzed in accordance with the chain of <br /> custody document. This analytical report must be reproduced in its entirety. <br /> Laboratory Representative Page of 18 <br />