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07/03/2007 11:58 FAX 4084515050 CLEAN HARBORS ENV. SRV. 121018/021 <br /> Excelchem Environmental Labs <br /> CLS Environmental Project: Flying J-Ripon <br /> 8 Crow Canyon Rd,Suite 205 Project Number: FJI-1 17 Date Reported: <br /> San Ramon,CA 94583 Project Manager: Travis Springer 12/06/06 16:30 <br /> SemiVolatile Organic Compounds by GC/MS- Quality Control <br /> Re rain ggpik our a °/oR$C �pL) <br /> Analyte Result p�imi Units Lev eel Resu�t %REC Limits RPD Limit Notes <br /> Batch APK0119-EPA 8270C <br /> Blank_(_APK0119-BLKI) _ _ Prepared&Analyzed: 11/21/06 _ <br /> Acenaphthene _ ND 2.0 ug/I <br /> 3-Nitroaniline ND 2.0 " <br /> 2,4-Dinitrophenol ND 2.0 " <br /> Dibenzofuran ND 2.0 " <br /> 2,4-Dinitrotoluene ND 2.0 <br /> 4-Nitrophenol ND 2.0 " <br /> Fluorene ND 2.0 " <br /> 4-Chlorophenyl phenyl ether ND 2.0 " <br /> Diethyl phthalate ND 2.0 " <br /> 4-Nitroaniline ND 2.0 " <br /> Azobenzene ND 2.0 " <br /> 4,6-Dinitro-2-methyl phenol ND 2.0 " <br /> N-Nitrosodiphenylamine ND 2.0 " <br /> 4-Bromophenyl phenyl ether ND 2.0 " <br /> Hexachlorobenzene ND 2.0 " <br /> Pentachlorophenol ND 2.0 " <br /> Phenanthrene ND 2.0 " <br /> Anthracene ND 2.0 " <br /> Carbazole ND 2.0 " <br /> Di-n-butyl phthalate ND 2.0 <br /> Fluoranthene ND 2.0 " <br /> Benzidine ND 2.0 <br /> Pyrene ' ND 2.0 " <br /> Butyl benzyl phthalate ND 2.0 " <br /> 3,3'-Dichlorobenzidine ND 2.0 " <br /> Benzo(a)anthracene ND 2.0 " <br /> Chrysene ND 2.0 " <br /> Bis(2-ethylhexyl)phthalate ND 2.0 <br /> Di-n-octyl phthalate ND 2.0 " <br /> Benzo(b)fluoranthene ND 2.0 " <br /> Benzo(k)fluoranthene ND 2.0 " <br /> Benzo(a)pyrene ND 2.0 " <br /> Indeno(1,2,3-cd)pyrene ND 2.0 " <br /> Dibenz(ah)anthracene ND 2.0 " <br /> Benzo(g,h,i)perylene ND 2.0 " <br /> Excelchem Environmental Lab. The results in this report apply to the samples analyzed in accordance with the chain of• <br /> custody document. This analytical report must be reproduced in its entirety. <br /> Laboratory Representative Page 16 of 18 <br />