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MATRIX SPIKE AND DUPLICATE RESULTS SUMMARY <br /> Login Number: C31148 <br /> Account: ENCOCALA - Encon Solutions, Inc. <br /> Project: 1145 S. Aurora Street - Stockton, CA <br /> QC Batch ID: MP7073 Methods: SW846 6010B <br /> Matrix Type: SOLID Units: mg/kg <br /> Prep Date: 12/03/13 <br /> C31148-7 Spikelot QC <br /> Metal Original MS MPIR4A o Rea Limits <br /> Aluminum <br /> Antimony am <br /> Arsenic 1.8 42.1 44.2 91.1 75-125 <br /> Barium 134 139 44.2 22.6N(a) 75-125 <br /> Beryllium our CD <br /> Boron <br /> N <br /> N <br /> Cadmium 0.0 40.8 44.2 92.2 75-125 <br /> Calcium •• <br /> Chromium 25.4 70.1 44.2 99.7 75-125 <br /> Cobalt our <br /> Copper our <br /> Iron <br /> Lead 4.6 56.5 44.2 111.6 75-125 <br /> Magnesium <br /> Manganese <br /> Molybdenum am <br /> Nickel am <br /> Potassium <br /> Selenium 1.7 40.0 44.2 86.6 75-125 <br /> Silicon <br /> Silver 0.21 37.5 44.2 84.3 75-125 <br /> Sodium <br /> Strontium <br /> Thallium our <br /> Tin <br /> Titanium <br /> Vanadium our <br /> Zinc our <br /> Associated samples M27073: C31148-5, C31148-7, C31148-11, C31148-15 <br /> Results < IDL are shown as zero for calculation purposes <br /> (1) Outside of QC limits <br /> (N) Matrix Spike Rec. outside of QC limits <br /> (anr) Analyte not requested <br /> (a) Spike recovery indicates possible matrix interference and/or sample nonhomogeneity. <br /> Page 1 <br /> ■ 77 of 80 <br /> R��tJT��T <br /> C31148 <br />