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ASSOCIATED LABORATORIES <br /> QA REPORT MRAY <br />'*ample G3 - LFBO113.00- S <br /> tatrix WATER <br /> Irep Date 01/13/00 <br /> Analysis Date 01/14/00 <br /> ID#'s in Batch LR 47067 <br /> IIATRIX SPIKE/MATRIX SPIKE DUPLICATE RESULT <br /> Reporting Units W mg/L <br /> Sample Spike Matrix Matrix %Ree %Rec <br /> Test Method Result Added ]-_§Rike S k Du MS MSD RPD <br /> TPH 8015D ND 5 573 527 115 105 8 4 <br />�1 D=riot Detected <br /> RPD=Relative Percent Difference of Haim Spike and+blatrtr Spike Duplicate %REC LI VITS = 70 - 130 <br /> 10 WS& AISD= Percent Recotiery of tlatrir Spike& llatrix Spike Duplicate IRPDLIiVITS = 30 <br /> REPARATION BLANK/ LAB CONTROL SAMPLE RESULTS <br /> PREP SLK JLCS <br /> 1 Value Result True %Rec L Limit H Limit <br /> ND 1090 10 109 80% 120% <br /> 4 =Aot Applicable <br /> CS Res ull=Lab Control.Sample Result <br /> True = True value of LCS <br /> Lnnit/H Limit=LCS Control Limits <br /> 01/26/2000 8015d_tph_0113w x1s <br /> I <br />