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ASSOCIATED LABORATORIES <br /> QA REPORT FORM[ - ORGANICS <br /> tSample LR 35861 -564 <br /> j'Pnx WATER <br /> Prep Date r 04/08/99 <br /> Inalysis Date 04/08/99 <br /> #'s in Batch LR 35842, 35852, 35861 <br /> TRIX SPIKE/MATRIX SPIKE DUPLICATE RESULT <br /> Reporting Units= mg/L <br /> Sample Spike Matrix Matrix %Rec %Ree <br /> Test Method Result ND Added Spike S ike Dup MS MSD RPD <br /> TPH 8015M-C350 U 200 242 239 12i 0 119 5 1 <br /> %REC LIMITS = 70 - 130 <br /> t_ "U"-Not Detected IRPDLIMITS = 30 <br /> RPD=Relative Percent Difference of Matrix Spike and Matrix Spike Duplicate <br /> w&MSD=Percent Recovery of Matrix Spike&Matrix Spike Duplicate <br /> tEPARATION BLANK/LAB CONTROL SAMPLE RESULTS <br /> 1 PREP BLANK LCS <br /> Value ND Result I True j %Rec I L Lunn I H Limit <br /> 50 U 309 300 1030 80% 120% <br /> value=Preparation Blank Value ND= "U"for Not-Detected <br /> fS Result=Lab Control Sample Result <br /> e=Prue Value of LCS <br /> Limit/H Limit=LCS Control Limits <br /> 4/22/99 8015m-g tph 0408W As <br />