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CLIENT- Secor Internattonai,Inc ANALYTICAL QC SUMMARY REPORT <br /> Work Order: 079296 <br /> Project CAL-Trans,940T 43148 00 TestCode: 8260OX10WP <br /> a m <br /> Sample ID A101305MB3 SampType MBLK TestCode 8260OX10WP Units pglL Prep Date Run ID MS11_051013A <br /> � y <br />! n- Client ID 27ZZZ Batch ID A05VW317 TestNo 8260+OX Analysis Date 1011312005 SegNo 810198 <br /> � o <br /> Analyte Result PQL SPK value SPK Ref Val %REC Lowl-imd HighLimt RPD Ref Val %RPD RPDLimct Qual <br /> 1,2-Dibromoethane NO 050 <br /> 1,2-Dichloroethane ND 050 <br /> Benzene NO 050 <br /> ti Di-isopropyl ether NO 0 50 <br /> Ethyl tert butyl ether NO 050 <br /> Ethylbenzene NO 0 50 <br /> m,p-Xylene ND 10 <br /> MTBE NO 0 50 <br /> a o-Xylene NO 0 50 <br /> Tert-amyl methyl ether NO 050 <br /> Tert-Butanol NO 10 <br /> Toluene NO 050 <br /> Surr 1,2-Dichloroethane-4 2867 0 25 0 115 83 126 0 0 <br /> Surr 4-Bromofluorobernzene 2859 0 25 0 114 84 129 0 0 <br /> :Z Surr Dibromofluorom ethane 24 88 0 25 0 995 84 118 0 0 <br /> Z. <br /> Sun-Toluene-d8 2547 0 25 0 102 92 124 0 0 <br /> A <br /> Sample ED A101405M83 SampType MBLK TestCode 8260OX10WP Units pg1L Prep Date Run lD MS11_051014A <br /> o Client ID 27777 Batch ID A05VW318 TestNo 8260+OX Analysis Date 1011412005 SegNo 810506 <br /> Ln <br /> Analyte Result PQL SPK value SPK Ref Val %REC LowLimit HighLimit RPD Ref Val %RPD RPDL)mit Qual <br /> cp <br /> 1,2-0ibramoethane ND 050 <br /> 01 <br /> 1,2-Dichloroethane ND 050 <br /> k" Benzene NO 050 <br /> 00 Di-isopropyl ether NO 0 50 <br /> q Ethyl tert-butyl ether NO 0 50 <br /> 2 Ethylbenzene NO 050 <br /> m,p-Xylene NO 10 <br /> MTBE NO 050 <br /> n <br /> k <br /> 0-Xylene NO 050 <br /> N <br /> Qualifiers ND-Not Detected at the Aeportmg Irmrt S-Spike Recovery outside accepted recovery hauls DO-Surrogate dilute out <br /> 1P1-Analyte detected below quantitation hmtts B-Analyte defected m the associated Method Blank H-Sample exceeded holding time <br /> O <br /> R-RPD outside accepted recovery limits Cafcutatrons are based an raw values Page 4 of 7 <br /> da <br /> Page 22 of 25 <br />