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Quality Report of Control <br /> P <br /> Pace Analytical Services, Inc. - New Orleans <br /> Organic Protocol- Single Batch <br /> Episode OLG <br /> Method Water GUMS Volatile Organics Batch 27937 Units <br /> Parameter Name LCS LCS LCSD MS MS MSD RPD QC Limits RPD Qu <br /> Spike %Rec %Rec Spike %Ree %Rec % LCS MS/MSD Max <br /> 1 Acetone(2-Propanone,Dimethyl ketone) 500 81 500 55 61 10 1-200 1-200 50 <br /> Benzene 500 97 500 101 95 6 76-127 76-127 ll <br /> Bromodichloromethane 500 100 Soo 102 96 5 1-200 1-200 50 <br /> Bromoform 500 100 500 94 86 9 1-200 1-200 50 <br /> Bromomethane(Methyl bromide) Soo 92 Soo 87 90 4 1-200 1-200 50 <br /> 2-Butanone(Methyl ethyl ketone) 500 82 500 65 64 2 1-200 1-200 50 <br /> Carbon dtsulfide 50 0 87 50 0 89 90 2 1-200 1-200 50 <br /> Carbon tetrachloride Soo 113 Soo 116 107 8 1-200 1-200 50 <br /> Chlorobenzene 500 98 500 l01 97 4 75-130 75-130 13 <br /> Chloroethane 500 96 500 91 88 4 1-200 1-200 50 <br /> Chloroform 50 0 95 500 99 95 4 1-200 1-200 50 <br /> Chloromethane(Methyl chloride) 500 114 500 104 111 6 1-200 1-200 50 <br /> Dtbromochloromethane 500 98 Soo 96 91 6 1-200 1-200 50 <br /> 1,1-Dichloroethane 500 96 500 98 95 3 1-200 1-200 50 <br /> 1,2-Dichloroethane(Ethylene dichloride) 50 0 105 Soo 102 95 8 1-200 1-200 50 <br /> 001-Dichloroethene(Dichloroethylene) 500 100 S00 100 101 I 61-145 61-145 l4 <br /> 2-Dichloroethene(total) 100 95 100 100 94 7 1-200 1-200 50 <br /> ,,2-Dichlompropane 50 0 98 500 100 95 6 1-200 1-200 50 <br /> cis-1,3-Dichloropropene 500 95 500 96 92 4 1-200 1-200 50 <br /> 1 trans-1,3-Dichloropropene 500 96 50 0 90 86 5 1-200 1-200 50 <br /> Ethylbenzene 500 104 500 108 100 8 1-200 1 200 50 <br /> 2-Hexanone 50 0 95 500 68 69 2 1-200 1 200 50 <br /> Methylene chloride(Dichloromethane) 50 0 71 500 66 64 3 1-200 1 200 SO <br /> 4-Methyl-2 pentanone(MIBK) 50 0 95 500 45 45 0 1-200 1-200 50 <br /> Styrene 50 0 98 500 98 88 10 1-200 1-200 50 <br /> 1,1,2,2-Tetrachloroethane 500 92 500 67 71 5 1-200 1-200 50 <br /> Tetrachloroethene(Perchloroethylene) Soo 95 500 107 95 12 1-200 1-200 50 <br /> Toluene 500 95 500 106 95 11 76-125 76-125 13 <br /> 1,1,1-Tnchloroethane(Methyl chloroform) 500 103 500 103 101 2 1-200 1-200 50 <br /> l 1,2-Tnchloroethane 500 95 500 91 82 10 1-200 1-200 50 <br /> Trichloroethene(Tnchloroethylene) 500 98 500 104 96 8 71-120 71-120 14 <br /> Vmyl chloride(Chloroethene) 500 89 50 0 83 89 7 1-200 1-200 50 <br /> Xylene(total) 150 103 150 106 102 4 1-200 1-200 50 <br /> 33 compaundisi reported <br /> *denotes recovery outside of QC limits <br /> MS spike concentrations are not corrected for moisture content of the spiked sample <br /> 10113199 17 09 17 <br />