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' Pace Analytical Services, Inc <br /> 1455 McDowell Blvd North Suite D <br /> Petaluma,CA 94954 <br /> Tel 707-792-1865 <br /> Fax 707-792-0342 <br /> DATE 03/31/98 <br /> PAGE 19 <br /> Pace Project Number 7010897 <br /> Client Project ID Stockton Yard <br /> e Sample No 701294217 Date Collected 03/16/98 Matrix Mater <br /> lent Sample ID MW 7 Date Received 03/17/98 <br /> fameters Results /Units PRL Analyzed Analyst CASK Footnotes <br /> i� Volatiles <br /> GAS/BTEX, Water Method EPA 8015M/8020M Prep Method EPA 8015M/8020M <br /> Gasoline ND ug/L 50 03/24/98 ADS <br /> Benzene NO ug/L 0 5 03/24/98 ADS 71-43 2 <br /> Toluene ND ug/L 0 5 03/24/98 ADS 108-88 3 <br /> Ethylbenzene NO ug/L 0 5 03/24/98 ADS 100-41 4 <br /> ' Xylene (Total) NO ug/L 1 03/24/98 ADS 1330-20-7 <br /> Methyl tert butyl Ether NO ug/L 5 03/24/98 ADS 1634-04-4 <br /> a a a Trifluorotoluene (S) 98 X 03/24/98 ADS 2164-17-2 <br /> 4 Bromafl uorobenzene (S) 82 X 03/24/98 ADS 460-00 4 <br /> GC Semi-VOA <br /> Rien Water by 8015 Modified Method TPH by EPA 8015H Prep Method EPA 3520 <br /> sel Fuel 0 13 mg/L 0 05 03/26/98 HCR 11-84 7 2 <br /> Motor Oil NO mg/L 0 25 03/26/98 HCR <br /> ' o Terphenyl (S) 60 % 03/26/98 HCR 84-15 1 <br /> n Pentacosane (S) 52 X 03/26/98 HCR 629-99 2 <br /> Date Extracted 03/21/98 <br /> IMS VOA <br /> /MS VOCs by 8260 Method EPA 8260 Prep Method EPA 8260 <br /> Dichlorodifluoromethane ND ug/L 5 03/26/98 AXM 75-71 8 <br /> Chloromethane NO ug/L 5 03/26/98 AXM 74 87 3 <br /> Vinyl Chloride ND ug/L 5 03/26/98 AXM 75 01-4 <br /> Bromomethane ND ug/L 5 03/26/98 AXM 74 83-9 <br /> Chloroethane NO ug/L 5 03/26/98 AXM 75-00 3 <br /> Trichlorofluoromethane NO ug/L 5 03/26/98 AXM 75-69-4 <br /> 1 Methylene Chloride ND ug/L 5 03/26/98 AXM 75-09 2 <br /> 1 1 Dichloroethene NO ug/L 5 03/26/98 AXM 75-35 4 <br /> trans-1,2 Dichloroethene NO ug/L 5 03/26/98 AXM 156-60 5 <br /> 1,1 Dichloroethane NO ug/L 5 03/26/98 AXM 75 34-3 <br /> 2 2-Dichloropropane NO ug/L 5 03/26/98 AXM 594 20-7 <br /> cis 1 2 Dichloroethene ND ug/L 5 03/26/98 AXM 156 59-2 <br /> Chloroform NO ug/L 5 03/26/98 AXM 67-66 3 <br /> ' Bromochloromethane ND ug/L 5 03/26/98 AXM 74-97 5 <br /> 1,1,1 Trichloroethane NO ug/L 5 03/26/98 AXM 71 55 6 <br /> REPORT OF LABORATORY ANALYSIS <br /> ' This report shall not be reproduced,except in full, <br /> without the written consent of Pace Analytical Services Inc <br />