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' ASSOCIATED LABORATORIES <br /> QA REPORT FORM - INORGANICS <br /> Sample LR 39152 -243 <br /> ratrix WATER <br /> Prep Date 06/30/99 <br /> Analysis Date 07/01/99 <br />�D#'s in Batch LR 39152, 39153, 39199,39215,39231 <br /> ATRIX SPIKE/MATRIX SPIKE DUPLICATE RESULT <br /> eporting Units= mg/L <br /> Sample Spike Matrix Matrix %Rec %Rec <br /> Test Method Result ND Added I Spike S k Dup MS MSD RPD <br /> TPH 8015D 0 0 U 330 290 280 879 848 3 5 <br /> %REC L1,V1TS = 70=- 13=0 ] <br /> ND= "U"-Not Detected RPD LIMITS = 30 <br /> D=Relative Pel cent Difference of Matrix Spike and Xfatrcr Spike Duplicate <br /> %PEC-MS&MSD=Percent Recovery of Matrix Spike&Matrix Spike Duplicate <br /> ft <br /> REPARATION BLANK/LAB CONTROL SAMPLE RESULTS <br /> PREP BLANK LCS <br /> Value ND Result True I %Rec I L Limit H Limit <br /> 00 U 560 670 836 80% 120% <br /> Ulue=Preparation Blank Value ND= "U"for Not-Detected <br /> S Result=Lab Control Sample Result <br /> True =True balue of LCS <br /> Limit/H Limit=LCS Control Limits <br /> 7113199 8015d_tph_0630w As <br />