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A s • Volatile Hydrocarbons by GUMS in Water Reporting Spike Source %REC RPD Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes Batch B000490-EPA 5030 GC/MS Blank(B000490-BLKI) __ Prepared 01/16/06 Analyzed 01/18/06 Benzene ND 10 ug/L Toluene ND 10 ug/L Ethylbenzene ND 10 ug/L m,p-Xylene ND 10 ug/L o-Xylene ND 10 ug/L Ethanol ND 10 ug/L Tertiary Butyl Alcohol (TBA) ND 25 ug/L Methyl tert-Butyl Ether (MTBE) ND 1 0 ug/L Di-isopropyl Ether (DIPS) ND 1 0 ug/L Ethyl tert-Butyl Ether (ETBE) ND 1 0 ug/L Tert-Amyl Methyl Ether (TAME) ND 10 ug/L Surrogate Debi omofluoromethane 196 uglL 200 98 70-130 Surrogate Toluene-d8 19 7 ug/L 200 98 70-130 Surrogate 4-Bromofluorobenzene 202 uglL 200 101 70-130 Latrix Spike(B000490-MSI) Source 6011312-01 Prepared 01/16/06 Analyzed 01/18/06 �1-Dichloroethene(1,1-DCE) 25 3 1 0 ug/L 250 ND 101 70-130 Benzene 25 1 1 0 ug/L 250 ND 100 70-130 Trichloroethene(TCE) 246 1 0 ug/L 250 ND 98 70-130 Toluene 24 8 1 0 ug/L 250 ND 99 70-130 Chlorobenzene 242 1 0 ug/L 25 0 ND 97 70-130 Surrogate Dibromofluoromethane 201 ug/L 200 100 70-130 Surrogate Toluene-d8 200 ug/L 200 100 70-130 Surrogate 4-Bromofluorobenzene 196 ug/L 200 98 70-130 Matrix Spike Dup(B000490-MSD1) Source 6011312-01 Prepared 01/16/06 Analyzed 01/18/06 1,1-Dichloroethene(1,1-DCE) 243 1 0 ug/L 25 0 ND 97 70-130 4 20 Benzene 243 1 0 ug/L 25 0 ND 97 70-130 3 20 Trichloroethene(TCE) 23 8 10 ug/L 25 0 ND 95 70-130 3 20 Toluene 23 9 1 0 ug/L 250 ND 96 70-130 3 20 Chlorobenzene 235 1 0 ug/L 250 ND 94 70-130 3 20 Surrogate Drbromofluoromethane 201 ug/L 200 100 70-130 Surrogate Toluene-d8 201 ug/L 200 100 70-130 Surrogate 4-Bromofluorobenzene 19 6 ug/L 200 98 70-130 • Page 4 of 6 Lab Protect# 6011603 CA Lab Accreditation # 2303