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North Coast Laboratories, Ltd. Date: 14-Nov-03 <br /> CLIENT: Alpha Analytical QC SUMMARY REPORT <br /> Work Order: 0311059 <br /> Laboratory Control Spike <br /> Project: KLF03110342 <br /> Sample ID LCS-10242 Batch ID: 10242 Test Code: 81405 Units: pglg Analysis Date 11/11/03 10:06:02 PM Prep Dale 1116103 <br /> Client ID: Run ID: ORGC13_031111A SegNo: 382947 <br /> Analyte Result Limit SPK value SPK Ref Val %Rec Lowl-imit Hight-imit RPD Ref Val %RPD RPDLimit Qual <br /> Dichlorvos 3.590 0.50 2.50 0 144% 46 145 0 <br /> Wevinphos 5.080 1.0 5.00 0 102% 32 131 0 <br /> Ethoprophos 5.240 1.0 5.00 0 105% 38 135 0 <br /> Phorate 2.626 1.0 2.50 0 105% 39 146 0 <br /> Demeton-S 9.194 2.0 10.0 0 91.9% 30 137 0 <br /> Diazinon 2.372 0.50 2.50 0 94.9% 42 132 0 <br /> Disulfolon 2.409 0.50 2.50 0 96.3% 37 139 0 <br /> Dimethoate 8.302 2.0 10.0 0 83.0% 17 134 0 <br /> Ronnel 2.538 0.50 2.50 0 102% 32 172 0 <br /> Methyl Parathion 1.050 0.50 2.50 0 42.0% 27 141 0 <br /> Chlorpyrifos 2.313 0.50 2.50 0 92.5% 37 150 0 <br /> Malathion 1.168 0.50 2.50 0 46.7% 48 139 0 S <br /> Parathion 2.190 0.50 2.50 0 87.6% 28 152 0 <br /> Fenthion 2.552 0.50 2.50 0 102% 37 137 0 <br /> Tetrachlorvinphos 2.532 0.50 2.50 0 101% 44 135 0 <br /> Ethion 2.343 0.50 2.50 0 93.7% 51 128 0 <br /> Fensulfothion 4.475 1.0 5.00 0 89.5% 20 138 0 <br /> Inphos 12.92 2.5 12.5 0 103% 38 146 0 <br /> umaphos 11.03 2.5 12.5 0 88.3% 39 143 0 <br /> Triphenylphosphate 5.10 0.10 5.00 0 102% 30 137 0 <br /> Qualifiers: ND-Not Detected at the Reporting Limit S-Spike Recovery outside accepted recovery limits 8-Analyte detected in the associated Method Blank <br /> 1-Analyte detected below quantitation limits R-RPD outside accepted recovery limits <br />